(R)-2-{(S)-2-[2-((4aR,6S,7R,8R,8aS)-7-Acetylamino-6-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy)-propionylamino]-propionylamino}-pentanedioic acid diamide

Base Information

Chemical Name:(R)-2-{(S)-2-[2-((4aR,6S,7R,8R,8aS)-7-Acetylamino-6-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy)-propionylamino]-propionylamino}-pentanedioic acid diamide
CAS No.:63092-13-7
Molecular Formula:C₃₃H₄₃N₅O₁₀
Molecular Weight:669.732
Hs Code.:

(R)-2-{(S)-2-[2-((4aR,6S,7R,8R,8aS)-7-Acetylamino-6-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy)-propionylamino]-propionylamino}-pentanedioic acid diamide

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Chemical Property of (R)-2-{(S)-2-[2-((4aR,6S,7R,8R,8aS)-7-Acetylamino-6-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy)-propionylamino]-propionylamino}-pentanedioic acid diamide

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Technology Process of (R)-2-{(S)-2-[2-((4aR,6S,7R,8R,8aS)-7-Acetylamino-6-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy)-propionylamino]-propionylamino}-pentanedioic acid diamide

There total 10 articles about (R)-2-{(S)-2-[2-((4aR,6S,7R,8R,8aS)-7-Acetylamino-6-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy)-propionylamino]-propionylamino}-pentanedioic acid diamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 76502-94-8
1-O-benzyl-4,6-O-benzylidene-N-acetylmuramyl-alanyl-D-isoglutamine methyl ester

: 63092-13-7,68199-64-4
1-O-benzyl-4,6-O-benzylidene-N-acetylmuramyl-alanyl-D-glutamic acid diamide

Guidance literature:: With ammonia; In methanol; for 144h; Ambient temperature;

Reference yield:

: 13343-63-0
benzyl 4,6-O-benzylidene-2-acetylamino-2-deoxy-α-D-glucopyranoside

: 63092-13-7,68199-64-4
1-O-benzyl-4,6-O-benzylidene-N-acetylmuramyl-alanyl-D-glutamic acid diamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1. Na-K alloy, NaI; 2. NaOH / 1. heating, 1 h, THF; 2. heating, 1 h, H₂O, methanol

2: 1. ethyl chloroformate, N-ethylmorpholine / 1. DMF, DMSO

With N-ethylmorpholine;; sodium hydroxide; potassium Sodium; chloroformic acid ethyl ester; sodium iodide;