Technology Process of C39H40O11
There total 5 articles about C39H40O11 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
acetone;
for 12h;
Inert atmosphere;
Schlenk technique;
Reflux;
DOI:10.1002/chem.201400157
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 12.17 h / 0 - 50 °C / Inert atmosphere; Schlenk technique
2: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 °C / Reflux; Inert atmosphere
3: triphenylphosphine; carbon tetrabromide / tetrahydrofuran / 24.17 h / 0 - 20 °C / Inert atmosphere; Schlenk technique
4: potassium carbonate / acetone / 12 h / Inert atmosphere; Schlenk technique; Reflux
With
lithium aluminium tetrahydride; carbon tetrabromide; di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine;
In
tetrahydrofuran; acetone;
1: |Mitsunobu Displacement;
DOI:10.1002/chem.201400157
- Guidance literature:
-
Multi-step reaction with 3 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 °C / Reflux; Inert atmosphere
2: triphenylphosphine; carbon tetrabromide / tetrahydrofuran / 24.17 h / 0 - 20 °C / Inert atmosphere; Schlenk technique
3: potassium carbonate / acetone / 12 h / Inert atmosphere; Schlenk technique; Reflux
With
lithium aluminium tetrahydride; carbon tetrabromide; potassium carbonate; triphenylphosphine;
In
tetrahydrofuran; acetone;
DOI:10.1002/chem.201400157
