DIOXO(PHENYL)(3-PHENYL-2-PROPENYL)-LAMBDA6-SULFANE

Base Information

• Chemical Name: DIOXO(PHENYL)(3-PHENYL-2-PROPENYL)-LAMBDA6-SULFANE
• CAS No.: 16212-07-0
• Molecular Formula: C15H14 O2 S
• Molecular Weight: 258.341
• Hs Code.: 2904100000
• Mol file: 16212-07-0.mol

Synonyms:Benzene,[(3-phenyl-2-propenyl)sulfonyl]-, (E)-; Benzene,[[(2E)-3-phenyl-2-propenyl]sulfonyl]- (9CI); Sulfone, cinnamyl phenyl, (E)-(8CI); [[(2E)-3-Phenyl-2-propenyl]sulfonyl]benzene

Chemical Property of DIOXO(PHENYL)(3-PHENYL-2-PROPENYL)-LAMBDA6-SULFANE

Chemical Property:

• Melting Point: 110-111 °C
• Boiling Point: 460.3±38.0 °C(Predicted)
• PSA: 42.52000
• Density: 1.192±0.06 g/cm3(Predicted)
• LogP: 4.25450

Purity/Quality:

99% ^*data from raw suppliers

DIOXO(PHENYL)(3-PHENYL-2-PROPENYL)-LAMBDA-6-SULFANE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of DIOXO(PHENYL)(3-PHENYL-2-PROPENYL)-LAMBDA6-SULFANE

There total 43 articles about DIOXO(PHENYL)(3-PHENYL-2-PROPENYL)-LAMBDA6-SULFANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

Cinnamyl acetate (21040-45-9) + sodium benzenesulfonate (873-55-2) → trans-cinnamyl phenyl sulfone (16212-07-0)

Guidance literature:

With trisodium tris(3-sulfophenyl)phosphine; 1-ethyl-3-methylimidazolium tetrafluoroborate; palladium diacetate; In water; for 0.025h; microwave irradiation;

DOI:10.1016/j.tetlet.2005.04.002

Reference yield: 99.0%

(allylsulfonyl)benzene (16212-05-8) + diphenyliodonium hexafluorophosphate (58109-40-3) → trans-cinnamyl phenyl sulfone (16212-07-0)

Guidance literature:

With palladium diacetate; sodium hydrogencarbonate; In acetonitrile; at 50 ℃; for 22h;

DOI:10.1021/ol9010739

Reference yield: 94.0%

sodium benzenesulfonate (873-55-2) + (2E)-3-phenyl-2-propen-1-ol (4407-36-7) → trans-cinnamyl phenyl sulfone (16212-07-0)

Guidance literature:

With palladium diacetate; triethyl borane; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide; at 80 ℃; for 12h;

DOI:10.1021/jo0505728

upstream raw materials:

(E)-1-phenyl-3-(phenylthio)propene

Cinnamyl acetate

sodium benzenesulfonate

Cinnamyl bromide

Downstream raw materials:

C₁₆H₁₄F₂O₂S

3-phenyl-1,5-hexadiene

(E)-1-phenyl-1,5-hexadiene

allylbenzene

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