5-bromo-thiophene-2-carboxylicacid[4-(1,1-dioxo-1lambda-6-thiomorpholin-4-ylmethyl)-phenyl]-amide

Base Information

Chemical Name:5-bromo-thiophene-2-carboxylicacid[4-(1,1-dioxo-1lambda-*6*-thiomorpholin-4-ylmethyl)-phenyl]-amide
CAS No.:1132825-60-5
Molecular Formula:C₁₆H₁₇BrN₂O₃S₂
Molecular Weight:429.359
Hs Code.:

Synonyms:5-bromo-thiophene-2-carboxylicacid[4-(1,1-dioxo-1lambda-*6*-thiomorpholin-4-ylmethyl)-phenyl]-amide

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Chemical Property of 5-bromo-thiophene-2-carboxylicacid[4-(1,1-dioxo-1lambda-*6*-thiomorpholin-4-ylmethyl)-phenyl]-amide

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Technology Process of 5-bromo-thiophene-2-carboxylicacid[4-(1,1-dioxo-1lambda-*6*-thiomorpholin-4-ylmethyl)-phenyl]-amide

There total 1 articles about 5-bromo-thiophene-2-carboxylicacid[4-(1,1-dioxo-1lambda-*6*-thiomorpholin-4-ylmethyl)-phenyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 31555-60-9
5-bromothiophene-2-carbonyl chloride

: 263339-24-8
4-(1,1-dioxo-1lambda* 6 *-thiomorpholin-4-ylmethyl)-phenylamine

: 1132825-60-5
5-bromo-thiophene-2-carboxylicacid[4-(1,1-dioxo-1lambda-*6*-thiomorpholin-4-ylmethyl)-phenyl]-amide

Guidance literature:: With triethylamine; In dichloromethane; for 16h;

Reference yield: 69.0%

: 1132825-58-1
[4-methyl-3-(4,4,5,5-tetramethyl-[l,3,2]dioxaborolan-2-yl)-phenyl]-carbamic acid tert-butyl ester

: 1132825-60-5
5-bromo-thiophene-2-carboxylicacid[4-(1,1-dioxo-1lambda-*6*-thiomorpholin-4-ylmethyl)-phenyl]-amide

: 1132825-62-7
3-{5-[4-(1.1-dioxo-1lambda-*6*-thiomorpholin-4-ylmethyl)-phenylcarbamoyl]-thiophen-2-yl}-4-methyl-phenyl-carbamic acid tert-butyl ester

Guidance literature:: With caesium carbonate; In 1,2-dimethoxyethane; water; at 85 ℃; for 16h;

Reference yield:

: 1132825-60-5
5-bromo-thiophene-2-carboxylicacid[4-(1,1-dioxo-1lambda-*6*-thiomorpholin-4-ylmethyl)-phenyl]-amide

: 1132825-64-9
5-(5-amino-2-methyl-phenyl)-thiophene-2-carboxylic acid [4-(1.1-dioxo-1lambda-* 6 *-thiomorpholm-4-ylmethyl)-phenyl]-amide

Guidance literature:: Multi-step reaction with 2 steps

1.1: caesium carbonate / 1,2-dimethoxyethane; water / 16 h / 85 °C

2.1: trifluoroacetic acid / dichloromethane / 2 h

2.3: pH 10

With caesium carbonate; trifluoroacetic acid; In 1,2-dimethoxyethane; dichloromethane; water;