3,4,5-tris(2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyl-oxy)ethoxy)ethoxy)ethoxy)benzyl alcohol

Base Information

• Chemical Name: 3,4,5-tris(2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyl-oxy)ethoxy)ethoxy)ethoxy)benzyl alcohol
• CAS No.: 1096159-41-9
• Molecular Formula: C₁₁₈H₂₀₆O₄₉
• Molecular Weight: 2408.9

Synonyms:3,4,5-tris(2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyl-oxy)ethoxy)ethoxy)ethoxy)benzyl alcohol

Chemical Property of 3,4,5-tris(2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyl-oxy)ethoxy)ethoxy)ethoxy)benzyl alcohol

Chemical Property:

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Technology Process of 3,4,5-tris(2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyl-oxy)ethoxy)ethoxy)ethoxy)benzyl alcohol

There total 1 articles about 3,4,5-tris(2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyl-oxy)ethoxy)ethoxy)ethoxy)benzyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

3,4,5-tris(2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyl-oxy)ethoxy)ethoxy)ethoxy)benzoic acid (1096159-40-8) → 3,4,5-tris(2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyl-oxy)ethoxy)ethoxy)ethoxy)benzyl alcohol (1096159-41-9)

Guidance literature:

3,4,5-tris(2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyl-oxy)ethoxy)ethoxy)ethoxy)benzoic acid; With 4-methyl-morpholine; chloroformic acid ethyl ester; In tetrahydrofuran; at -15 ℃; for 1h; Inert atmosphere;

With sodium tetrahydroborate; In tetrahydrofuran; at -5 - 25 ℃; for 4h; Inert atmosphere;

DOI:10.1039/b811464a

Reference yield: 83.0%

3,4,5-tris(2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyl-oxy)ethoxy)ethoxy)ethoxy)benzyl alcohol (1096159-41-9) + Methacryloyl chloride (920-46-7,26937-45-1) → 3,4,5-tris(2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyl-oxy)ethoxy)ethoxy)ethoxy)benzyl methacrylate (1096159-42-0)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 0 - 25 ℃; for 5.08333h; Inert atmosphere;

DOI:10.1039/b811464a

Reference yield: 72.0%

3,4,5-tris(2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyl-oxy)ethoxy)ethoxy)ethoxy)benzyl alcohol (1096159-41-9) → 3,4,5-tris(2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyl-oxy)ethoxy)ethoxy)ethoxy)benzyl chloride

Guidance literature:

With dmap; thionyl chloride; In dichloromethane; at 20 ℃; Inert atmosphere;

DOI:10.1039/b814192d

upstream raw materials:

3,4,5-tris(2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyl-oxy)ethoxy)ethoxy)ethoxy)benzoic acid

Downstream raw materials:

3,4,5-tris(2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyl-oxy)ethoxy)ethoxy)ethoxy)benzyl methacrylate

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