3,4,5-tris(2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyl-oxy)ethoxy)ethoxy)ethoxy)benzoic acid

Base Information

• Chemical Name: 3,4,5-tris(2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyl-oxy)ethoxy)ethoxy)ethoxy)benzoic acid
• CAS No.: 1096159-40-8
• Molecular Formula: C₁₁₈H₂₀₄O₅₀
• Molecular Weight: 2422.89
• Mol file: 1096159-40-8.mol

Synonyms:3,4,5-tris(2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyl-oxy)ethoxy)ethoxy)ethoxy)benzoic acid

Chemical Property of 3,4,5-tris(2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyl-oxy)ethoxy)ethoxy)ethoxy)benzoic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,4,5-tris(2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyl-oxy)ethoxy)ethoxy)ethoxy)benzoic acid

There total 2 articles about 3,4,5-tris(2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyl-oxy)ethoxy)ethoxy)ethoxy)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

C119H206O50 (1202396-91-5) → 3,4,5-tris(2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyl-oxy)ethoxy)ethoxy)ethoxy)benzoic acid (1096159-40-8)

Guidance literature:

With lithium hydroxide monohydrate; In methanol; at -5 - 20 ℃; for 3h;

DOI:10.1039/c5ra22224a

Reference yield: 50.0%

1-(hydroxymethyl)-3,4,5-tri{2-[2-(2-ethoxyethoxy)ethoxy]ethoxy}benzene (1096159-35-1) + C47H62O20S3 (1005214-34-5) → 3,4,5-tris(2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyl-oxy)ethoxy)ethoxy)ethoxy)benzoic acid (1096159-40-8)

Guidance literature:

With 15-crown-5; sodium hydride; potassium iodide; In tetrahydrofuran; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.1039/b811464a

Reference yield: 81.0%

3,4,5-tris(2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyl-oxy)ethoxy)ethoxy)ethoxy)benzoic acid (1096159-40-8) → 3,4,5-tris(2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyl-oxy)ethoxy)ethoxy)ethoxy)benzyl alcohol (1096159-41-9)

Guidance literature:

3,4,5-tris(2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyl-oxy)ethoxy)ethoxy)ethoxy)benzoic acid; With 4-methyl-morpholine; chloroformic acid ethyl ester; In tetrahydrofuran; at -15 ℃; for 1h; Inert atmosphere;

With sodium tetrahydroborate; In tetrahydrofuran; at -5 - 25 ℃; for 4h; Inert atmosphere;

DOI:10.1039/b811464a

upstream raw materials:

1-(hydroxymethyl)-3,4,5-tri{2-[2-(2-ethoxyethoxy)ethoxy]ethoxy}benzene

C₄₇H₆₂O₂₀S₃

C₁₁₉H₂₀₆O₅₀

Downstream raw materials:

3,4,5-tris(2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyl-oxy)ethoxy)ethoxy)ethoxy)benzyl alcohol

1-adamantyl 3,4,5-tris(2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyloxy)ethoxy)ethoxy)ethoxy)benzamide