(2-methyl-5-tert-butylphenyl) 2-O-benzoyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

Base Information

Chemical Name:(2-methyl-5-tert-butylphenyl) 2-O-benzoyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside
CAS No.:1361016-60-5
Molecular Formula:C₃₁H₃₄O₆S
Molecular Weight:534.673
Hs Code.:

Synonyms:(2-methyl-5-tert-butylphenyl) 2-O-benzoyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

Suppliers and Price of (2-methyl-5-tert-butylphenyl) 2-O-benzoyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (2-methyl-5-tert-butylphenyl) 2-O-benzoyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (2-methyl-5-tert-butylphenyl) 2-O-benzoyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

There total 3 articles about (2-methyl-5-tert-butylphenyl) 2-O-benzoyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1361016-58-1
(2-methyl-5-tert-butylphenyl) 1-thio-α-D-mannopyranoside

: 1361016-60-5
(2-methyl-5-tert-butylphenyl) 2-O-benzoyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: (1S)-10-camphorsulfonic acid / dichloromethane / 5 h / 20 °C / Molecular sieve; Inert atmosphere

2.1: (1S)-10-camphorsulfonic acid / 1 h / 20 °C / Inert atmosphere

2.2: 1 h

With (1S)-10-camphorsulfonic acid; In dichloromethane;
DOI:10.1016/j.bmc.2011.12.048

Reference yield:

: 3458-28-4
D-Mannose

: 1361016-60-5
(2-methyl-5-tert-butylphenyl) 2-O-benzoyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine; acetic anhydride / 20 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: (1S)-10-camphorsulfonic acid / dichloromethane / 5 h / 20 °C / Molecular sieve; Inert atmosphere

3.1: (1S)-10-camphorsulfonic acid / 1 h / 20 °C / Inert atmosphere

3.2: 1 h

With pyridine; (1S)-10-camphorsulfonic acid; acetic anhydride; In dichloromethane;
DOI:10.1016/j.bmc.2011.12.048

Reference yield:

: 7340-90-1
2-methyl-5-tert-butylthiophenol

: 1361016-60-5
(2-methyl-5-tert-butylphenyl) 2-O-benzoyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine; acetic anhydride / 20 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: (1S)-10-camphorsulfonic acid / dichloromethane / 5 h / 20 °C / Molecular sieve; Inert atmosphere

3.1: (1S)-10-camphorsulfonic acid / 1 h / 20 °C / Inert atmosphere

3.2: 1 h

With pyridine; (1S)-10-camphorsulfonic acid; acetic anhydride; In dichloromethane;
DOI:10.1016/j.bmc.2011.12.048