4-((2S,6R)-6-(4-hydroxyphenylethyl)-5,6-dihydro-2H-pyran-2-yl)-2-nitrophenol

Base Information

Chemical Name:4-((2S,6R)-6-(4-hydroxyphenylethyl)-5,6-dihydro-2H-pyran-2-yl)-2-nitrophenol
CAS No.:1288996-91-7
Molecular Formula:C₁₉H₁₉NO₅
Molecular Weight:341.364
Hs Code.:

Synonyms:4-((2S,6R)-6-(4-hydroxyphenylethyl)-5,6-dihydro-2H-pyran-2-yl)-2-nitrophenol

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Chemical Property of 4-((2S,6R)-6-(4-hydroxyphenylethyl)-5,6-dihydro-2H-pyran-2-yl)-2-nitrophenol

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Technology Process of 4-((2S,6R)-6-(4-hydroxyphenylethyl)-5,6-dihydro-2H-pyran-2-yl)-2-nitrophenol

There total 2 articles about 4-((2S,6R)-6-(4-hydroxyphenylethyl)-5,6-dihydro-2H-pyran-2-yl)-2-nitrophenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1288996-84-8
4-((2S,6R)-6-(4-(tert-butyldimethylsilyloxy)phenylethyl)-5,6-dihydro-2H-pyran-2-yl)-2-nitrophenol

: 1288996-91-7
4-((2S,6R)-6-(4-hydroxyphenylethyl)-5,6-dihydro-2H-pyran-2-yl)-2-nitrophenol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jo2002787

Reference yield:

: 1202784-98-2
(R)-2-[4-(tert-butyldimethylsilyloxy)phenethyl]-3,4-dihydro-2H-pyran

: 1252036-52-4
4-hydroxy-3-nitrobenzenediazonium tetrafluoroborate

: 1288996-91-7
4-((2S,6R)-6-(4-hydroxyphenylethyl)-5,6-dihydro-2H-pyran-2-yl)-2-nitrophenol

Guidance literature:: Multi-step reaction with 2 steps

1: sodium acetate; palladium diacetate / acetonitrile / 20 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; sodium acetate; palladium diacetate; In tetrahydrofuran; acetonitrile; 1: Mizoroki-Heck reaction;
DOI:10.1021/jo2002787