C₄₀H₅₆N₂O₃Si

Base Information

Chemical Name:C₄₀H₅₆N₂O₃Si
CAS No.:1416273-59-0
Molecular Formula:C₄₀H₅₆N₂O₃Si
Molecular Weight:640.982
Hs Code.:

C<sub>40</sub>H<sub>56</sub>N<sub>2</sub>O<sub>3</sub>Si

Synonyms:C₄₀H₅₆N₂O₃Si

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Chemical Property of C₄₀H₅₆N₂O₃Si

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Technology Process of C₄₀H₅₆N₂O₃Si

There total 7 articles about C₄₀H₅₆N₂O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1416273-53-4
nonyl 3-amino-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate

: 1416273-57-8
3-bromo-5-{(4-[(triisopropylsilyl)ethynyl]phenoxy)methyl}aniline

: 1416273-59-0
C₄₀H₅₆N₂O₃Si

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; toluene; at 65 ℃; for 3h; Inert atmosphere;
DOI:10.1039/c2cc35974j

Reference yield:

: 6307-83-1
3-bromo-5-nitro-benzoic acid

: 1416273-59-0
C₄₀H₅₆N₂O₃Si

Guidance literature:: Multi-step reaction with 4 steps

1: dimethylsulfide borane complex / tetrahydrofuran / 6 h / -15 - 60 °C / Inert atmosphere

2: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 17.5 h / 0 - 20 °C

3: tin(II) chloride dihdyrate / ethanol / 2 h / 60 °C

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / toluene; water; tetrahydrofuran / 3 h / 65 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tin(II) chloride dihdyrate; dimethylsulfide borane complex; potassium carbonate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; ethanol; water; toluene; 2: |Mitsunobu Displacement / 4: |Suzuki Coupling;
DOI:10.1039/c2cc35974j

Reference yield:

: 121-92-6
3-nitrobenzoic acid

: 1416273-59-0
C₄₀H₅₆N₂O₃Si

Guidance literature:: Multi-step reaction with 5 steps

1: sulfuric acid; N-Bromosuccinimide / 3 h / 60 - 70 °C

2: dimethylsulfide borane complex / tetrahydrofuran / 6 h / -15 - 60 °C / Inert atmosphere

3: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 17.5 h / 0 - 20 °C

4: tin(II) chloride dihdyrate / ethanol / 2 h / 60 °C

5: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / toluene; water; tetrahydrofuran / 3 h / 65 °C / Inert atmosphere

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tin(II) chloride dihdyrate; dimethylsulfide borane complex; sulfuric acid; potassium carbonate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; ethanol; water; toluene; 3: |Mitsunobu Displacement / 5: |Suzuki Coupling;
DOI:10.1039/c2cc35974j