5(S)-tert-butyloxycarbonylamino-4(R)-(1'(R/S)-cyclohex-2'-enyl)-2,2-dimethyl-1,3-dioxan

Base Information

Chemical Name:5(S)-tert-butyloxycarbonylamino-4(R)-(1'(R/S)-cyclohex-2'-enyl)-2,2-dimethyl-1,3-dioxan
CAS No.:188659-63-4
Molecular Formula:C₁₇H₂₉NO₄
Molecular Weight:311.422
Hs Code.:

Synonyms:5(S)-tert-butyloxycarbonylamino-4(R)-(1'(R/S)-cyclohex-2'-enyl)-2,2-dimethyl-1,3-dioxan

Suppliers and Price of 5(S)-tert-butyloxycarbonylamino-4(R)-(1'(R/S)-cyclohex-2'-enyl)-2,2-dimethyl-1,3-dioxan

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5(S)-tert-butyloxycarbonylamino-4(R)-(1'(R/S)-cyclohex-2'-enyl)-2,2-dimethyl-1,3-dioxan

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 5(S)-tert-butyloxycarbonylamino-4(R)-(1'(R/S)-cyclohex-2'-enyl)-2,2-dimethyl-1,3-dioxan

There total 3 articles about 5(S)-tert-butyloxycarbonylamino-4(R)-(1'(R/S)-cyclohex-2'-enyl)-2,2-dimethyl-1,3-dioxan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 77-76-9
2,2-dimethoxy-propane

: 188659-56-5
2-(S)-tert-butyloxycarbonylamino-1-hydroxy-3-(R)-hydroxy-3-[1'(RS)-cyclohex-2'-enyl]propane

: 188659-63-4
5(S)-tert-butyloxycarbonylamino-4(R)-(1'(R/S)-cyclohex-2'-enyl)-2,2-dimethyl-1,3-dioxan

Guidance literature:: With toluene-4-sulfonic acid; In dichloromethane; Ambient temperature;
DOI:10.1016/S0040-4020(97)00050-1

Reference yield:

: 91103-36-5,157683-97-1
N-tert.-butyloxycarbonyl-L-serinal

: 188659-63-4
5(S)-tert-butyloxycarbonylamino-4(R)-(1'(R/S)-cyclohex-2'-enyl)-2,2-dimethyl-1,3-dioxan

Guidance literature:: Multi-step reaction with 2 steps

1: Sn / aq. ethanol / 6 h / 0 °C / sonication

2: 50 percent / p-TsOH / CH₂Cl₂ / Ambient temperature

With tin; toluene-4-sulfonic acid; In ethanol; dichloromethane;
DOI:10.1016/S0040-4020(97)00050-1

Reference yield:

: 1521-51-3,113667-32-6
rac-3-bromocyclohexene

: 188659-63-4
5(S)-tert-butyloxycarbonylamino-4(R)-(1'(R/S)-cyclohex-2'-enyl)-2,2-dimethyl-1,3-dioxan

Guidance literature:: Multi-step reaction with 2 steps

1: Sn / aq. ethanol / 6 h / 0 °C / sonication

2: 50 percent / p-TsOH / CH₂Cl₂ / Ambient temperature

With tin; toluene-4-sulfonic acid; In ethanol; dichloromethane;
DOI:10.1016/S0040-4020(97)00050-1