2,2',3,3'-Tetra-tert-butyl-1,1'-bicyclotriphosphan

Base Information

• Chemical Name: 2,2',3,3'-Tetra-tert-butyl-1,1'-bicyclotriphosphan
• CAS No.: 93646-62-9
• Molecular Formula: C₁₆H₃₆P₆
• Molecular Weight: 414.304

Synonyms:2,2',3,3'-Tetra-tert-butyl-1,1'-bicyclotriphosphan

Chemical Property of 2,2',3,3'-Tetra-tert-butyl-1,1'-bicyclotriphosphan

Chemical Property:

Purity/Quality:

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Technology Process of 2,2',3,3'-Tetra-tert-butyl-1,1'-bicyclotriphosphan

There total 2 articles about 2,2',3,3'-Tetra-tert-butyl-1,1'-bicyclotriphosphan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

1,2-di-tert-butyl-3-chloro-cyclotriphosphane (93646-64-1,103774-32-9) + 1,2-di-tert-butyl-3-trimethylstannyl-cyclotriphosphane (93646-63-0,103774-31-8) → trimethyltin(IV)chloride (1066-45-1) + 2,2',3,3'-Tetra-tert-butyl-1,1'-bicyclotriphosphan (93646-62-9)

Guidance literature:

at 13 ℃; 1) 1 h, -40 deg C, 2) 2 h, r. t.;

Reference yield:

1,2-di-tert-butyl-3-(dichlorophosphino)-cyclotriphosphane (103717-24-4) + 1,2-di-tert-butyl-1,2-bis(trimethylstannyl)diphosphane (103717-23-3) → trimethyltin(IV)chloride (1066-45-1) + 2,2',3,3'-Tetra-tert-butyl-1,1'-bicyclotriphosphan (93646-62-9)

Guidance literature:

Reference yield:

2,2',3,3'-Tetra-tert-butyl-1,1'-bicyclotriphosphan (93646-62-9) → tri-tert-butyl phosphine (13716-12-6) + 2,3,4,6-tetra-tert-butylbicyclo<3.1.0>hexaphosphane (79593-41-2) + 2,2',3,3',4,4'-hexa-tert-butyl-1,1'-bicyclotetraphosphane (77256-90-7,145678-98-4)

Guidance literature:

at 128 ℃;

upstream raw materials:

1,2-di-tert-butyl-3-chloro-cyclotriphosphane

1,2-di-tert-butyl-3-trimethylstannyl-cyclotriphosphane

1,2-di-tert-butyl-3-(dichlorophosphino)-cyclotriphosphane

1,2-di-tert-butyl-1,2-bis(trimethylstannyl)diphosphane

Downstream raw materials:

tri-tert-butyl phosphine

2,3,4,6-tetra-tert-butylbicyclo<3.1.0>hexaphosphane

2,2',3,3',4,4'-hexa-tert-butyl-1,1'-bicyclotetraphosphane

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