8-(p-azido-N-ethyl-tetrafluoroaniline)-3,7-dimethyl-1-acetoxyl-2,6-octadiene

Base Information

Chemical Name:8-(p-azido-N-ethyl-tetrafluoroaniline)-3,7-dimethyl-1-acetoxyl-2,6-octadiene
CAS No.:447454-16-2
Molecular Formula:C₂₀H₂₄F₄N₄O₂
Molecular Weight:428.43
Hs Code.:

Synonyms:8-(p-azido-N-ethyl-tetrafluoroaniline)-3,7-dimethyl-1-acetoxyl-2,6-octadiene

Suppliers and Price of 8-(p-azido-N-ethyl-tetrafluoroaniline)-3,7-dimethyl-1-acetoxyl-2,6-octadiene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 8-(p-azido-N-ethyl-tetrafluoroaniline)-3,7-dimethyl-1-acetoxyl-2,6-octadiene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 8-(p-azido-N-ethyl-tetrafluoroaniline)-3,7-dimethyl-1-acetoxyl-2,6-octadiene

There total 1 articles about 8-(p-azido-N-ethyl-tetrafluoroaniline)-3,7-dimethyl-1-acetoxyl-2,6-octadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 37905-02-5
(2E,6E)-3,7-dimethyl-8-oxoocta-2,6-dien-1-yl acetate

: 56553-60-7
sodium tris(acetoxy)borohydride

: 294187-78-3
p-azidotetrafluoroaniline

: 447454-16-2
8-(p-azido-N-ethyl-tetrafluoroaniline)-3,7-dimethyl-1-acetoxyl-2,6-octadiene

Guidance literature:: p-azidotetrafluoroaniline; With pyridine; titanium tetrachloride; In dichloromethane; toluene; at 20 ℃; for 0.0833333h;

(2E,6E)-3,7-dimethyl-8-oxoocta-2,6-dien-1-yl acetate; In dichloromethane; toluene; at 20 ℃; for 8h;

sodium tris(acetoxy)borohydride; With acetic acid; In dichloromethane; toluene; at 20 ℃; for 24h; Further stages.;
DOI:10.1021/ja0124717

Reference yield: 97.0%

: 447454-16-2
8-(p-azido-N-ethyl-tetrafluoroaniline)-3,7-dimethyl-1-acetoxyl-2,6-octadiene

: 447454-20-8
8-(p-azido-N-ethyl-tetrafluoroaniline)-3,7-dimethyl-2,6-octadien-1-ol

Guidance literature:: With potassium carbonate; In methanol; at 20 ℃;
DOI:10.1021/ja0124717

Reference yield:

: 447454-16-2
8-(p-azido-N-ethyl-tetrafluoroaniline)-3,7-dimethyl-1-acetoxyl-2,6-octadiene

: 447454-23-1
8-(p-azido-N-ethyl-tetrafluoroaniline)-3,7-dimethyl-1-chloro-2,6-octadiene

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / aq. potassium carbonate / methanol / 20 °C

2: 85 percent / N,N-diisopropylethylamine; dichlorotriphenylphosphorane / acetonitrile / 0.67 h / 0 °C

With potassium carbonate; N-ethyl-N,N-diisopropylamine; dichlorotriphenylphosphorane; In methanol; acetonitrile;
DOI:10.1021/ja0124717