6-(benzyloxy)-2-hexanone dimethylhydrazone

Base Information

Chemical Name:6-(benzyloxy)-2-hexanone dimethylhydrazone
CAS No.:80471-22-3
Molecular Formula:C₁₅H₂₄N₂O
Molecular Weight:248.368
Hs Code.:

Synonyms:6-(benzyloxy)-2-hexanone dimethylhydrazone

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Chemical Property of 6-(benzyloxy)-2-hexanone dimethylhydrazone

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Technology Process of 6-(benzyloxy)-2-hexanone dimethylhydrazone

There total 2 articles about 6-(benzyloxy)-2-hexanone dimethylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 13483-31-3
Acetone dimethylhydrazone

: 54314-84-0
1-[(3-bromopropoxy)methyl]-benzene

: 80471-22-3
6-(benzyloxy)-2-hexanone dimethylhydrazone

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; 1.) -78 deg C, 0.5 h, 2.) -78 deg C, 0.5 h; -78 deg C to 0 deg C, 1 h,; 25 deg C, 0.5 h;
DOI:10.1021/ja00368a024

Reference yield:

: 4799-68-2
3-benzyloxypropan-1-ol

: 80471-22-3
6-(benzyloxy)-2-hexanone dimethylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / triphenylphosphine, N-bromosuccinimide / 16 h / 25 °C

2: 68 percent / n-BuLi / tetrahydrofuran; hexane / 1.) -78 deg C, 0.5 h, 2.) -78 deg C, 0.5 h; -78 deg C to 0 deg C, 1 h,; 25 deg C, 0.5 h

With N-Bromosuccinimide; n-butyllithium; triphenylphosphine; In tetrahydrofuran; hexane;
DOI:10.1021/ja00368a024

Reference yield:

: 69060-78-2
2-(2-cyanoethyl)-5-methylcyclohex-2-en-1-one

: 80471-22-3
6-(benzyloxy)-2-hexanone dimethylhydrazone

: 80471-27-8,80471-28-9
(4RS,6SR)-6-<6-hydroxy-2-oxohexyl>-4-methyl-2-oxocyclohexanepropanenitrile

: 80471-25-6,80471-26-7
(4RS,6SR)-4-methyl-2-oxo-6-<2-oxo-6-(phenylmethoxy)hexyl>cyclohexanepropanenitrile

Guidance literature:: With copper(l) iodide; n-butyllithium; diisopropylsulfide; water; Yield given. Multistep reaction. Yields of byproduct given; 1.) hexane, THF, -78 deg C, 20 min, 2.) THF;
DOI:10.1021/ja00368a024