(4R,5R)-3-(2,2-dimethyl-5-phenylmethyl-1,3-dioxolan-4-yl)propyl 3,5-dinitrobenzoate

Base Information

Chemical Name:(4R,5R)-3-(2,2-dimethyl-5-phenylmethyl-1,3-dioxolan-4-yl)propyl 3,5-dinitrobenzoate
CAS No.:140844-92-4
Molecular Formula:C₂₂H₂₄N₂O₈
Molecular Weight:444.441
Hs Code.:

Synonyms:(4R,5R)-3-(2,2-dimethyl-5-phenylmethyl-1,3-dioxolan-4-yl)propyl 3,5-dinitrobenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4R,5R)-3-(2,2-dimethyl-5-phenylmethyl-1,3-dioxolan-4-yl)propyl 3,5-dinitrobenzoate

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Technology Process of (4R,5R)-3-(2,2-dimethyl-5-phenylmethyl-1,3-dioxolan-4-yl)propyl 3,5-dinitrobenzoate

There total 1 articles about (4R,5R)-3-(2,2-dimethyl-5-phenylmethyl-1,3-dioxolan-4-yl)propyl 3,5-dinitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 140844-91-3
(4R,5R)-3-(2,2-dimethyl-5-phenylmethyl-1,3-dioxolan-4-yl)propan-1-ol

: 99-33-2
3,5-dinitrobenoyl chloride

: 140844-92-4
(4R,5R)-3-(2,2-dimethyl-5-phenylmethyl-1,3-dioxolan-4-yl)propyl 3,5-dinitrobenzoate

Guidance literature:: With pyridine; dmap; for 1h; Ambient temperature;

Reference yield: 100.0%

: 140844-92-4
(4R,5R)-3-(2,2-dimethyl-5-phenylmethyl-1,3-dioxolan-4-yl)propyl 3,5-dinitrobenzoate

: 140844-91-3
(4R,5R)-3-(2,2-dimethyl-5-phenylmethyl-1,3-dioxolan-4-yl)propan-1-ol

Guidance literature:: With potassium hydroxide; In tetrahydrofuran; ethanol; for 0.333333h; Ambient temperature;

Reference yield:

: 140844-92-4
(4R,5R)-3-(2,2-dimethyl-5-phenylmethyl-1,3-dioxolan-4-yl)propyl 3,5-dinitrobenzoate

: 125225-54-9
(4R,5R)-5-hydroxy-6-phenyl-4-hexanolide

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / 2 N potassium hydroxide / ethanol; tetrahydrofuran / 0.33 h / Ambient temperature

2: 1.) oxalyl chloride, dimethyl sulfoxide, 2.) triethylamine / 1.) dichloromethane, -70 deg C, 1 h, 2.) dichloromethane, -> -10 deg C

3: AgNO₃, KOH, H₂O / methanol

4: conc. HCl

With hydrogenchloride; potassium hydroxide; oxalyl dichloride; water; silver nitrate; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; methanol; ethanol;