6,6'-[3-aza(2-methoxy-2-oxoethyl)penta-1,5-di-yl]-1',2,3,3',4,4'-hexa-O-benzylsucrose

Base Information

Chemical Name:6,6'-[3-aza(2-methoxy-2-oxoethyl)penta-1,5-di-yl]-1',2,3,3',4,4'-hexa-O-benzylsucrose
CAS No.:1415048-97-3
Molecular Formula:C₆₁H₆₉NO₁₃
Molecular Weight:1024.22
Hs Code.:

Synonyms:6,6'-[3-aza(2-methoxy-2-oxoethyl)penta-1,5-di-yl]-1',2,3,3',4,4'-hexa-O-benzylsucrose

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Chemical Property of 6,6'-[3-aza(2-methoxy-2-oxoethyl)penta-1,5-di-yl]-1',2,3,3',4,4'-hexa-O-benzylsucrose

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Technology Process of 6,6'-[3-aza(2-methoxy-2-oxoethyl)penta-1,5-di-yl]-1',2,3,3',4,4'-hexa-O-benzylsucrose

There total 3 articles about 6,6'-[3-aza(2-methoxy-2-oxoethyl)penta-1,5-di-yl]-1',2,3,3',4,4'-hexa-O-benzylsucrose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1415048-93-9
6,6'-(3-azapenta-1,5-di-yl)-1',2,3,3',4,4'-hexa-O-benzylsucrose

: 96-32-2
bromoacetic acid methyl ester

: 1415048-97-3
6,6'-[3-aza(2-methoxy-2-oxoethyl)penta-1,5-di-yl]-1',2,3,3',4,4'-hexa-O-benzylsucrose

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 4h;
DOI:10.1016/j.tetasy.2012.10.003 DOI:10.1016/j.tetasy.2012.10.003

Reference yield:

: 1415048-92-8
6-O-(2-aminoethyl)-1',2,3,3',4,4'-hexa-O-benzyl-6'-O-(2-hydroxyethyl)-sucrose

: 1415048-97-3
6,6'-[3-aza(2-methoxy-2-oxoethyl)penta-1,5-di-yl]-1',2,3,3',4,4'-hexa-O-benzylsucrose

Guidance literature:: Multi-step reaction with 2 steps

1.1: triphenylphosphine / toluene / 0.17 h / Reflux

1.2: 4 h / 80 °C / Reflux

2.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 100 °C

With potassium carbonate; triphenylphosphine; In N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.tetasy.2012.10.003 DOI:10.1016/j.tetasy.2012.10.003

Reference yield:

: 1186624-89-4
6-O-(cyanomethyl)-1',2,3,3',4,4'-hexa-O-benzylsucrose

: 1415048-97-3
6,6'-[3-aza(2-methoxy-2-oxoethyl)penta-1,5-di-yl]-1',2,3,3',4,4'-hexa-O-benzylsucrose

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrabutylammomium bromide; sodium hydroxide / water; toluene / 15 h / 20 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / -78 - 20 °C

3.1: triphenylphosphine / toluene / 0.17 h / Reflux

3.2: 4 h / 80 °C / Reflux

4.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 100 °C

With lithium aluminium tetrahydride; tetrabutylammomium bromide; potassium carbonate; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; water; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.tetasy.2012.10.003 DOI:10.1016/j.tetasy.2012.10.003