6-O-(2-aminoethyl)-1',2,3,3',4,4'-hexa-O-benzyl-6'-O-(2-hydroxyethyl)-sucrose

Base Information

Chemical Name:6-O-(2-aminoethyl)-1',2,3,3',4,4'-hexa-O-benzyl-6'-O-(2-hydroxyethyl)-sucrose
CAS No.:1415048-92-8
Molecular Formula:C₅₈H₆₇NO₁₂
Molecular Weight:970.169
Hs Code.:

Synonyms:6-O-(2-aminoethyl)-1',2,3,3',4,4'-hexa-O-benzyl-6'-O-(2-hydroxyethyl)-sucrose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-O-(2-aminoethyl)-1',2,3,3',4,4'-hexa-O-benzyl-6'-O-(2-hydroxyethyl)-sucrose

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Technology Process of 6-O-(2-aminoethyl)-1',2,3,3',4,4'-hexa-O-benzyl-6'-O-(2-hydroxyethyl)-sucrose

There total 1 articles about 6-O-(2-aminoethyl)-1',2,3,3',4,4'-hexa-O-benzyl-6'-O-(2-hydroxyethyl)-sucrose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1415048-91-7
1',2,3,3',4,4'-hexa-O-benzyl-6'-O-(2-tert-butoxy-2-oxoethyl)-6-O-cyanomethylsucrose

: 1415048-92-8
6-O-(2-aminoethyl)-1',2,3,3',4,4'-hexa-O-benzyl-6'-O-(2-hydroxyethyl)-sucrose

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at -78 - 20 ℃;
DOI:10.1016/j.tetasy.2012.10.003 DOI:10.1016/j.tetasy.2012.10.003

Reference yield:

: 1415048-92-8
6-O-(2-aminoethyl)-1',2,3,3',4,4'-hexa-O-benzyl-6'-O-(2-hydroxyethyl)-sucrose

: 1415048-93-9
6,6'-(3-azapenta-1,5-di-yl)-1',2,3,3',4,4'-hexa-O-benzylsucrose

Guidance literature:: 6-O-(2-aminoethyl)-1',2,3,3',4,4'-hexa-O-benzyl-6'-O-(2-hydroxyethyl)-sucrose; With triphenylphosphine; In toluene; for 0.166667h; Reflux;

With 1H-imidazole; iodine; In toluene; at 80 ℃; for 4h; Reflux;
DOI:10.1016/j.tetasy.2012.10.003 DOI:10.1016/j.tetasy.2012.10.003

Reference yield:

: 1415048-92-8
6-O-(2-aminoethyl)-1',2,3,3',4,4'-hexa-O-benzyl-6'-O-(2-hydroxyethyl)-sucrose

: 1415048-97-3
6,6'-[3-aza(2-methoxy-2-oxoethyl)penta-1,5-di-yl]-1',2,3,3',4,4'-hexa-O-benzylsucrose

Guidance literature:: Multi-step reaction with 2 steps

1.1: triphenylphosphine / toluene / 0.17 h / Reflux

1.2: 4 h / 80 °C / Reflux

2.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 100 °C

With potassium carbonate; triphenylphosphine; In N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.tetasy.2012.10.003 DOI:10.1016/j.tetasy.2012.10.003