cyclohexanesulfonic acid (3-bromo-2-cyanophenyl)methylamide

Base Information

• Chemical Name: cyclohexanesulfonic acid (3-bromo-2-cyanophenyl)methylamide
• CAS No.: 1430754-13-4
• Molecular Formula: C₁₄H₁₇BrN₂O₂S
• Molecular Weight: 357.271
• Mol file: 1430754-13-4.mol

Synonyms:cyclohexanesulfonic acid (3-bromo-2-cyanophenyl)methylamide

Chemical Property of cyclohexanesulfonic acid (3-bromo-2-cyanophenyl)methylamide

Chemical Property:

Purity/Quality:

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Technology Process of cyclohexanesulfonic acid (3-bromo-2-cyanophenyl)methylamide

There total 2 articles about cyclohexanesulfonic acid (3-bromo-2-cyanophenyl)methylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclohexanesulfonic acid methylamide (7010-85-7) + 2-bromo-6-fluorobenzonitrile (79544-27-7) → cyclohexanesulfonic acid (3-bromo-2-cyanophenyl)methylamide (1430754-13-4)

Guidance literature:

With potassium carbonate; In N,N-dimethyl acetamide; at 85 ℃; for 72h;

Reference yield:

cyclohexanesulfonyl chloride (4837-38-1) → cyclohexanesulfonic acid (3-bromo-2-cyanophenyl)methylamide (1430754-13-4)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran / 1 h / 20 °C

2: potassium carbonate / N,N-dimethyl acetamide / 72 h / 85 °C

With potassium carbonate; In tetrahydrofuran; N,N-dimethyl acetamide;

upstream raw materials:

cyclohexanesulfonic acid methylamide

2-bromo-6-fluorobenzonitrile

cyclohexanesulfonyl chloride

Refernces