(E)-N-(1-(4-methoxyphenyl)-5-oxohex-3-en-1-yl)-4-methylbenzenesulfonamide

Base Information

Chemical Name:(E)-N-(1-(4-methoxyphenyl)-5-oxohex-3-en-1-yl)-4-methylbenzenesulfonamide
CAS No.:1338441-53-4
Molecular Formula:C₂₀H₂₃NO₄S
Molecular Weight:373.473
Hs Code.:

Synonyms:(E)-N-(1-(4-methoxyphenyl)-5-oxohex-3-en-1-yl)-4-methylbenzenesulfonamide

Suppliers and Price of (E)-N-(1-(4-methoxyphenyl)-5-oxohex-3-en-1-yl)-4-methylbenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N-(1-(4-methoxyphenyl)-5-oxohex-3-en-1-yl)-4-methylbenzenesulfonamide

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Technology Process of (E)-N-(1-(4-methoxyphenyl)-5-oxohex-3-en-1-yl)-4-methylbenzenesulfonamide

There total 1 articles about (E)-N-(1-(4-methoxyphenyl)-5-oxohex-3-en-1-yl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 78-94-4,25038-87-3
methyl vinyl ketone

: 243671-18-3
N-[1-(4-methoxyphenyl)but-3-en-1-yl]-4-methylbenzenesulfonamide

: 1338441-53-4
(E)-N-(1-(4-methoxyphenyl)-5-oxohex-3-en-1-yl)-4-methylbenzenesulfonamide

Guidance literature:: With Hoveyda-Grubbs catalyst second generation; In dichloromethane; at 55 ℃; for 71h; Inert atmosphere;
DOI:10.1039/c1cc14257g

Reference yield:

: 1338441-53-4
(E)-N-(1-(4-methoxyphenyl)-5-oxohex-3-en-1-yl)-4-methylbenzenesulfonamide

: 1338441-76-1
2-(4-methoxyphenyl)-6-methyl-4-(p-tolyl)pyridine

Guidance literature:: Multi-step reaction with 3 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; N-Methyldicyclohexylamine; tri tert-butylphosphoniumtetrafluoroborate / toluene / 3 h / 80 °C / Inert atmosphere

2: trifluoroacetic acid / toluene / 2 h / 80 °C

3: 1,8-diazabicyclo[5.4.0]undec-7-ene / 7 h / 80 °C

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; N-Methyldicyclohexylamine; 1,8-diazabicyclo[5.4.0]undec-7-ene; trifluoroacetic acid; tri tert-butylphosphoniumtetrafluoroborate; In toluene; 1: Heck reaction;
DOI:10.1039/c1cc14257g

Reference yield:

: 1338441-53-4
(E)-N-(1-(4-methoxyphenyl)-5-oxohex-3-en-1-yl)-4-methylbenzenesulfonamide

: C₂₇H₂₇NO₃S

Guidance literature:: Multi-step reaction with 2 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; N-Methyldicyclohexylamine; tri tert-butylphosphoniumtetrafluoroborate / toluene / 3 h / 80 °C / Inert atmosphere

2: trifluoroacetic acid / toluene / 2 h / 80 °C

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; N-Methyldicyclohexylamine; trifluoroacetic acid; tri tert-butylphosphoniumtetrafluoroborate; In toluene; 1: Heck reaction;
DOI:10.1039/c1cc14257g