2,4-Di-O-benzyl-3-desoxy-3-(N-methylacetamido)-β-L-arabinopyranosylchlorid

Base Information

Chemical Name:2,4-Di-O-benzyl-3-desoxy-3-(N-methylacetamido)-β-L-arabinopyranosylchlorid
CAS No.:77881-71-1
Molecular Formula:C₂₂H₂₆ClNO₄
Molecular Weight:403.906
Hs Code.:

Synonyms:2,4-Di-O-benzyl-3-desoxy-3-(N-methylacetamido)-β-L-arabinopyranosylchlorid

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Chemical Property of 2,4-Di-O-benzyl-3-desoxy-3-(N-methylacetamido)-β-L-arabinopyranosylchlorid

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Technology Process of 2,4-Di-O-benzyl-3-desoxy-3-(N-methylacetamido)-β-L-arabinopyranosylchlorid

There total 1 articles about 2,4-Di-O-benzyl-3-desoxy-3-(N-methylacetamido)-β-L-arabinopyranosylchlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 40147-35-1,78085-61-7,78085-62-8,79298-79-6,79298-80-9
1-O-Acetyl-2,4-di-O-benzyl-3-desoxy-3-(N-methylacetamido)-L-arabinopyranose

: 77881-71-1
2,4-Di-O-benzyl-3-desoxy-3-(N-methylacetamido)-β-L-arabinopyranosylchlorid

Guidance literature:: With hydrogenchloride; acetyl chloride; In 1,4-dioxane; at 25 ℃; for 22.5h;
DOI:10.1039/P19810002151

Reference yield: 15.0%

: 42801-36-5
1,3,2',6'-tetrakis-N-benzyloxycarbonylgentamine C_1a

: 77881-71-1
2,4-Di-O-benzyl-3-desoxy-3-(N-methylacetamido)-β-L-arabinopyranosylchlorid

: 79248-85-4
O-2,4-di-O-benzyl-3-deoxy-3-N-methylacetamido-β-L-arabinopyranosyl-(1->6)-1,3,2',6'-tetrakis-N-benzyloxycarbonylgentamine C_1a

Guidance literature:: With silver(I) 4-methylbenzenesulfonate; In dichloromethane; at 25 ℃; for 21.25h;
DOI:10.1039/P19810002151

Reference yield:

: 77881-71-1
2,4-Di-O-benzyl-3-desoxy-3-(N-methylacetamido)-β-L-arabinopyranosylchlorid

: 56153-88-9,56272-23-2,61769-70-8,65207-16-1
O-3-deoxy-3-methylamino-β-L-arabinopyranosyl-(1->6)-gentamine C_1a

Guidance literature:: Multi-step reaction with 2 steps

1: 15 percent / silver toluene-p-sulphonate / CH₂Cl₂ / 21.25 h / 25 °C

2: 7 percent / ammonia, sodium / 6 h / -79 °C

With ammonia; silver(I) 4-methylbenzenesulfonate; sodium; In dichloromethane;
DOI:10.1039/P19810002151