1,N-dibenzoyl-4-(methylamino)-1,2,2a,3-tetrahydrobenzindole

Base Information

• Chemical Name: 1,N-dibenzoyl-4-(methylamino)-1,2,2a,3-tetrahydrobenzindole
• CAS No.: 100999-19-7
• Molecular Formula: C₂₆H₂₂N₂O₂
• Molecular Weight: 394.473

Synonyms:1,N-dibenzoyl-4-(methylamino)-1,2,2a,3-tetrahydrobenzindole

Chemical Property of 1,N-dibenzoyl-4-(methylamino)-1,2,2a,3-tetrahydrobenzindole

Chemical Property:

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Technology Process of 1,N-dibenzoyl-4-(methylamino)-1,2,2a,3-tetrahydrobenzindole

There total 3 articles about 1,N-dibenzoyl-4-(methylamino)-1,2,2a,3-tetrahydrobenzindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-benzoyl-1,2,2a,3-tetrahydrobenzindol-4-(5H)-one (51867-06-2) + benzoyl chloride (98-88-4) → 1,N-dibenzoyl-4-(methylamino)-1,2,2a,3-tetrahydrobenzindole (100999-19-7)

Guidance literature:

With ammonia; triethylamine; In diethyl ether; dichloromethane; carbon dioxide;

Reference yield:

1-benzoyl-1,2,2a,3-tetrahydrobenzindol-4-(5H)-one (51867-06-2) → 1,N-dibenzoyl-4-(methylamino)-1,2,2a,3-tetrahydrobenzindole (100999-19-7)

Guidance literature:

Multi-step reaction with 2 steps

1: Montmorillonite K₁₀ (acidic catalyst) / diethyl ether / 2 h / Ambient temperature

2: Et₃N / CH₂Cl₂ / 14 h / Ambient temperature

With Montmorillonite K₁₀ (acidic catalyst); triethylamine; In diethyl ether; dichloromethane;

DOI:10.1021/jm00105a047

Reference yield:

1-benzoyl-4-methylamino-1,2,2a,3-tetrahydrobenzindole (74607-02-6) + benzoyl chloride (98-88-4) → 1,N-dibenzoyl-4-(methylamino)-1,2,2a,3-tetrahydrobenzindole (100999-19-7)

Guidance literature:

With triethylamine; In dichloromethane; for 14h; Ambient temperature;

DOI:10.1021/jm00105a047

upstream raw materials:

1-benzoyl-4-methylamino-1,2,2a,3-tetrahydrobenzindole

benzoyl chloride

1-benzoyl-1,2,2a,3-tetrahydrobenzindol-4-(5H)-one

Downstream raw materials:

(5aS^*,6aR^*,12bR^*)-4-benzoyl-4,5,5a,6,6a,7,8,12b-octahydro-8-oxo-7-methylindolo<4,3-ab>phenanthridine

(+/-)-trans-4,6,6a,7,8,12b-hexahydro-7-methylindolo<4,3-ab>phenanthridine

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