(2R)-N-<(2S)-5--2-<amino>pentanoyl>bornane-10,2-sultam

Base Information

Chemical Name:(2R)-N-<(2S)-5--2-<amino>pentanoyl>bornane-10,2-sultam
CAS No.:161264-09-1
Molecular Formula:C₃₂H₄₃N₃O₆S₄
Molecular Weight:693.974
Hs Code.:

(2R)-N-<(2S)-5-<N-(benzyloxy)-N-tosylamino>-2-<<bis(methylthio)methylidene>amino>pentanoyl>bornane-10,2-sultam

Synonyms:(2R)-N-<(2S)-5--2-<amino>pentanoyl>bornane-10,2-sultam

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Chemical Property of (2R)-N-<(2S)-5--2-<amino>pentanoyl>bornane-10,2-sultam

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Technology Process of (2R)-N-<(2S)-5--2-<amino>pentanoyl>bornane-10,2-sultam

There total 4 articles about (2R)-N-<(2S)-5--2-<amino>pentanoyl>bornane-10,2-sultam which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1576-39-2
O-benzyl-N-tosylhydroxylamine

: 161264-04-6
(2R)-N-<(2S)-2-<amino>-5-chloropentan-1-oyl>bornane-10.2-sultam

: 161264-09-1
(2R)-N-<(2S)-5--2-<amino>pentanoyl>bornane-10,2-sultam

Guidance literature:: With potassium hexamethylsilazane; In tetrahydrofuran; at 65 ℃; for 5h;
DOI:10.1002/hlca.19940770823

Reference yield:

: 58091-08-0
methyl N-(bis(methyl)thiomethilene)glycinate

: 161264-09-1
(2R)-N-<(2S)-5--2-<amino>pentanoyl>bornane-10,2-sultam

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / Me₃Al / hexane; toluene / 24 h / 50 °C

2: 72.4 percent / BuLi / hexane; tetrahydrofuran; various solvent(s) / 3 h / Ambient temperature

3: 83 percent / KN(SiMe₃)2 / tetrahydrofuran; various solvent(s) / 5 h / 65 °C

With n-butyllithium; trimethylaluminum; potassium hexamethylsilazane; In tetrahydrofuran; hexane; toluene;
DOI:10.1002/hlca.19940770823

Reference yield:

: 127556-03-0
(2R)-N-{N'-[bis(methylthio)methylidine]glycyl}bornane-10,2-sultam

: 161264-09-1
(2R)-N-<(2S)-5--2-<amino>pentanoyl>bornane-10,2-sultam

Guidance literature:: Multi-step reaction with 2 steps

1: 72.4 percent / BuLi / hexane; tetrahydrofuran; various solvent(s) / 3 h / Ambient temperature

2: 83 percent / KN(SiMe₃)2 / tetrahydrofuran; various solvent(s) / 5 h / 65 °C

With n-butyllithium; potassium hexamethylsilazane; In tetrahydrofuran; hexane;
DOI:10.1002/hlca.19940770823