6-[5-(4-chloro-phenyl)-[1,2,4]oxadiazol-3-ylmethoxy]-indan-1-yl-chloride

Base Information

Chemical Name:6-[5-(4-chloro-phenyl)-[1,2,4]oxadiazol-3-ylmethoxy]-indan-1-yl-chloride
CAS No.:935248-17-2
Molecular Formula:C₁₈H₁₄Cl₂N₂O₂
Molecular Weight:361.227
Hs Code.:

Synonyms:6-[5-(4-chloro-phenyl)-[1,2,4]oxadiazol-3-ylmethoxy]-indan-1-yl-chloride

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Chemical Property of 6-[5-(4-chloro-phenyl)-[1,2,4]oxadiazol-3-ylmethoxy]-indan-1-yl-chloride

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Technology Process of 6-[5-(4-chloro-phenyl)-[1,2,4]oxadiazol-3-ylmethoxy]-indan-1-yl-chloride

There total 4 articles about 6-[5-(4-chloro-phenyl)-[1,2,4]oxadiazol-3-ylmethoxy]-indan-1-yl-chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 6-[5-(4-chloro-phenyl)-[1,2,4]oxadiazol-3-ylmethoxy]-indan-1-ol

: 935248-17-2
6-[5-(4-chloro-phenyl)-[1,2,4]oxadiazol-3-ylmethoxy]-indan-1-yl-chloride

Guidance literature:: With thionyl chloride; In toluene; at 20 - 60 ℃; for 1.5h;
DOI:10.1016/j.bmcl.2006.12.109

Reference yield:

: 13623-25-1
6-methoxy-2,3-dihydro-1H-inden-1-one

: 935248-17-2
6-[5-(4-chloro-phenyl)-[1,2,4]oxadiazol-3-ylmethoxy]-indan-1-yl-chloride

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / aluminum chloride / toluene / 0.5 h / Heating

2: 63 percent / potassium carbonate / tetrabutylammonium iodide / acetonitrile / 40 h / 60 - 65 °C

3: 100 percent / sodium borohydride / methanol / 1 h / 20 °C

4: 100 percent / thionyl chloride / toluene / 1.5 h / 20 - 60 °C

With sodium tetrahydroborate; aluminium trichloride; thionyl chloride; potassium carbonate; tetra-(n-butyl)ammonium iodide; In methanol; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2006.12.109

Reference yield:

: 62803-47-8
6-hydroxy-1-indanone

: 935248-17-2
6-[5-(4-chloro-phenyl)-[1,2,4]oxadiazol-3-ylmethoxy]-indan-1-yl-chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 63 percent / potassium carbonate / tetrabutylammonium iodide / acetonitrile / 40 h / 60 - 65 °C

2: 100 percent / sodium borohydride / methanol / 1 h / 20 °C

3: 100 percent / thionyl chloride / toluene / 1.5 h / 20 - 60 °C

With sodium tetrahydroborate; thionyl chloride; potassium carbonate; tetra-(n-butyl)ammonium iodide; In methanol; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2006.12.109