N^α-benzyloxycarbonyl,N^α-methyl-N^ε-tert-butoxycarbonyl,N^ε-methyl-L-lysine

Base Information

Chemical Name:N^α-benzyloxycarbonyl,N^α-methyl-N^ε-tert-butoxycarbonyl,N^ε-methyl-L-lysine
CAS No.:128719-76-6
Molecular Formula:C₂₁H₃₂N₂O₆
Molecular Weight:408.495
Hs Code.:

N<sup>α</sup>-benzyloxycarbonyl,N<sup>α</sup>-methyl-N<sup>ε</sup>-tert-butoxycarbonyl,N<sup>ε</sup>-methyl-L-lysine

Synonyms:N^α-benzyloxycarbonyl,N^α-methyl-N^ε-tert-butoxycarbonyl,N^ε-methyl-L-lysine

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Chemical Property of N^α-benzyloxycarbonyl,N^α-methyl-N^ε-tert-butoxycarbonyl,N^ε-methyl-L-lysine

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Technology Process of N^α-benzyloxycarbonyl,N^α-methyl-N^ε-tert-butoxycarbonyl,N^ε-methyl-L-lysine

There total 1 articles about N^α-benzyloxycarbonyl,N^α-methyl-N^ε-tert-butoxycarbonyl,N^ε-methyl-L-lysine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2389-60-8
Z-Lys(Boc)-OH

: 74-88-4
methyl iodide

: 128719-76-6
N^α-benzyloxycarbonyl,N^α-methyl-N^ε-tert-butoxycarbonyl,N^ε-methyl-L-lysine

Guidance literature:: With sodium hydride; Yield given. Multistep reaction;

Reference yield: 73.0%

: 128719-76-6
N^α-benzyloxycarbonyl,N^α-methyl-N^ε-tert-butoxycarbonyl,N^ε-methyl-L-lysine

: 68762-02-7
(S)-2-[(R)-2-Amino-3-(1H-indol-3-yl)-propionylamino]-4-methyl-pentanoic acid methyl ester; hydrochloride

: 128719-77-7
N^α-benzyloxycarbonyl,N^α-methyl-L-lysyl(N^ε-Me,N^ε-Boc)-D-tryptophyl-L-leucine methyl ester

Guidance literature:: With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 4 ℃;

Reference yield:

: 128719-76-6
N^α-benzyloxycarbonyl,N^α-methyl-N^ε-tert-butoxycarbonyl,N^ε-methyl-L-lysine

: 128719-79-9
N-benzyloxycarbonyl-D-phenylalanyl-N^α-methyl-L-lysyl(N^ε-Me,Boc)-D-tryptophyl-L-leucine methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / dicyclohexylcarbodiimide (DCCI), 1-hydroxybenzotriazole (HOBt), Et₃N / dimethylformamide / 4 °C

2: H₂, glacial acetic acid / 5percent Pd/C

3: Et₃N / dimethylformamide / 1.) -10 deg C, 30 min, 2.) 4 deg C, 2 h

With hydrogen; benzotriazol-1-ol; acetic acid; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In N,N-dimethyl-formamide;