1-(4-bromophenyl)-3-hexyl-1H-imidazolium bis(trifluoromethanesulfonyl)amide

Base Information

Chemical Name:1-(4-bromophenyl)-3-hexyl-1H-imidazolium bis(trifluoromethanesulfonyl)amide
CAS No.:1286795-92-3
Molecular Formula:C₂F₆NO₄S₂*C₁₅H₂₀BrN₂
Molecular Weight:588.39
Hs Code.:

Synonyms:1-(4-bromophenyl)-3-hexyl-1H-imidazolium bis(trifluoromethanesulfonyl)amide

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Chemical Property of 1-(4-bromophenyl)-3-hexyl-1H-imidazolium bis(trifluoromethanesulfonyl)amide

Chemical Property:

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Technology Process of 1-(4-bromophenyl)-3-hexyl-1H-imidazolium bis(trifluoromethanesulfonyl)amide

There total 4 articles about 1-(4-bromophenyl)-3-hexyl-1H-imidazolium bis(trifluoromethanesulfonyl)amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1176198-59-6
1-(4-bromophenyl)-3-hexyl-1H-imidazolium bromide

: 90076-65-6
bis(trifluoromethane)sulfonimide lithium

: 1286795-92-3
1-(4-bromophenyl)-3-hexyl-1H-imidazolium bis(trifluoromethanesulfonyl)amide

Guidance literature:: In methanol; dichloromethane; water; at 20 ℃; for 24h;
DOI:10.1002/chem.202102545

Reference yield:

: 106-40-1
4-bromo-aniline

: 1286795-92-3
1-(4-bromophenyl)-3-hexyl-1H-imidazolium bis(trifluoromethanesulfonyl)amide

Guidance literature:: Multi-step reaction with 4 steps

1.1: methanol; water / 20 °C

2.1: ammonium chloride / methanol; water / 1 h / Reflux

2.2: 4 h / Reflux

2.3: pH 9

3.1: tetrahydrofuran / 20 h / 95 °C / pressure tube

4.1: dichloromethane; water / 20 °C

With ammonium chloride; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1002/asia.201000744

Reference yield:

: C₈H₆BrNO

: 1286795-92-3
1-(4-bromophenyl)-3-hexyl-1H-imidazolium bis(trifluoromethanesulfonyl)amide

Guidance literature:: Multi-step reaction with 3 steps

1.1: ammonium chloride / methanol; water / 1 h / Reflux

1.2: 4 h / Reflux

1.3: pH 9

2.1: tetrahydrofuran / 20 h / 95 °C / pressure tube

3.1: dichloromethane; water / 20 °C

With ammonium chloride; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1002/asia.201000744