BF₂(NC₄H(CH₃)2)2CC₆H₃OCH₃C₂H

Base Information

Chemical Name:BF₂(NC₄H(CH₃)2)2CC₆H₃OCH₃C₂H
CAS No.:1260102-23-5
Molecular Formula:C₂₂H₂₁BF₂N₂O
Molecular Weight:378.229
Hs Code.:

BF<sub>2</sub>(NC<sub>4</sub>H(CH<sub>3</sub>)2)2CC<sub>6</sub>H<sub>3</sub>OCH<sub>3</sub>C<sub>2</sub>H

Synonyms:BF₂(NC₄H(CH₃)2)2CC₆H₃OCH₃C₂H

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Chemical Property of BF₂(NC₄H(CH₃)2)2CC₆H₃OCH₃C₂H

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Technology Process of BF₂(NC₄H(CH₃)2)2CC₆H₃OCH₃C₂H

There total 6 articles about BF₂(NC₄H(CH₃)2)2CC₆H₃OCH₃C₂H which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: C₂₅H₃₁BF₂N₂OSi

: 1260102-23-5
BF₂(NC₄H(CH₃)2)2CC₆H₃OCH₃C₂H

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at -78 ℃; for 0.0833333h; Inert atmosphere;
DOI:10.1021/ja107193j

Reference yield:

: 16870-28-3
4-iodosalicylic acid

: 1260102-23-5
BF₂(NC₄H(CH₃)2)2CC₆H₃OCH₃C₂H

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium carbonate / acetone / 20 h / 60 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / tetrahydrofuran / -78 - 25 °C / Inert atmosphere

3.1: pyridinium chlorochromate / dichloromethane / 2 h / 25 °C / Inert atmosphere

4.1: trifluoroacetic acid / dichloromethane / 1.5 h / 25 °C / Inert atmosphere

4.2: 0.67 h / 25 °C

5.1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / tetrahydrofuran / 12 h / 25 °C / Inert atmosphere

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.08 h / -78 °C / Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; potassium carbonate; triethylamine; pyridinium chlorochromate; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1021/ja107193j

Reference yield:

: 139102-37-7
4-iodo-2-methoxybenzaldehyde

: 1260102-23-5
BF₂(NC₄H(CH₃)2)2CC₆H₃OCH₃C₂H

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluoroacetic acid / dichloromethane / 1.5 h / 25 °C / Inert atmosphere

1.2: 0.67 h / 25 °C

2.1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / tetrahydrofuran / 12 h / 25 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.08 h / -78 °C / Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutyl ammonium fluoride; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja107193j