2-(4-benzhydryl-1-piperazinylmethyl)-6,7-dimethoxy-1,2,3,4-tetrahydro-1-naphthalenol hydrogen fumarate

Base Information

Chemical Name:2-(4-benzhydryl-1-piperazinylmethyl)-6,7-dimethoxy-1,2,3,4-tetrahydro-1-naphthalenol hydrogen fumarate
CAS No.:65472-81-3
Molecular Formula:C₄H₄O₄*C₃₀H₃₆N₂O₃
Molecular Weight:588.701
Hs Code.:

Synonyms:2-(4-benzhydryl-1-piperazinylmethyl)-6,7-dimethoxy-1,2,3,4-tetrahydro-1-naphthalenol hydrogen fumarate

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Chemical Property of 2-(4-benzhydryl-1-piperazinylmethyl)-6,7-dimethoxy-1,2,3,4-tetrahydro-1-naphthalenol hydrogen fumarate

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Technology Process of 2-(4-benzhydryl-1-piperazinylmethyl)-6,7-dimethoxy-1,2,3,4-tetrahydro-1-naphthalenol hydrogen fumarate

There total 5 articles about 2-(4-benzhydryl-1-piperazinylmethyl)-6,7-dimethoxy-1,2,3,4-tetrahydro-1-naphthalenol hydrogen fumarate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 110-17-8,26099-09-2
(2E)-but-2-enedioic acid

: 65503-06-2
2-(4-benzhydryl-piperazin-1-ylmethyl)-6,7-dimethoxy-3,4-dihydro-2H-naphthalen-1-one

: 65472-81-3,88284-73-5
(1S,2S)-2-(4-Benzhydryl-piperazin-1-ylmethyl)-6,7-dimethoxy-1,2,3,4-tetrahydro-naphthalen-1-ol; compound with (E)-but-2-enedioic acid

Guidance literature:: With sodium tetrahydroborate; In methanol; chloroform; for 0.5h; Ambient temperature;
DOI:10.1248/cpb.31.2006

Reference yield:

: 110-17-8,26099-09-2
(2E)-but-2-enedioic acid

: 65503-06-2
2-(4-benzhydryl-piperazin-1-ylmethyl)-6,7-dimethoxy-3,4-dihydro-2H-naphthalen-1-one

: 65472-81-3
2-(4-benzhydryl-1-piperazinylmethyl)-6,7-dimethoxy-1,2,3,4-tetrahydro-1-naphthalenol hydrogen fumarate

Guidance literature:: With sodium borohydrid; In methanol; diethyl ether; chloroform; water;

Reference yield:

: 13575-75-2
6,7-dimethoxy-1-oxo-1,2,3,4-tetrahydronaphthalene

: 65472-81-3,88284-73-5
(1S,2S)-2-(4-Benzhydryl-piperazin-1-ylmethyl)-6,7-dimethoxy-1,2,3,4-tetrahydro-naphthalen-1-ol; compound with (E)-but-2-enedioic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 44 percent / ethanol / Ambient temperature

2: 36 percent / NaBH₄ / methanol; CHCl₃ / 0.5 h / Ambient temperature

With sodium tetrahydroborate; In methanol; ethanol; chloroform;
DOI:10.1248/cpb.31.2006