(2R,3S,4R,5R,6R)-2-Hydroxymethyl-6-(4-methoxy-phenyl)-tetrahydro-pyran-3,4,5-triol

Base Information

Chemical Name:(2R,3S,4R,5R,6R)-2-Hydroxymethyl-6-(4-methoxy-phenyl)-tetrahydro-pyran-3,4,5-triol
CAS No.:117772-56-2
Molecular Formula:C₁₃H₁₈O₆
Molecular Weight:270.282
Hs Code.:

Synonyms:(2R,3S,4R,5R,6R)-2-Hydroxymethyl-6-(4-methoxy-phenyl)-tetrahydro-pyran-3,4,5-triol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3S,4R,5R,6R)-2-Hydroxymethyl-6-(4-methoxy-phenyl)-tetrahydro-pyran-3,4,5-triol

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Technology Process of (2R,3S,4R,5R,6R)-2-Hydroxymethyl-6-(4-methoxy-phenyl)-tetrahydro-pyran-3,4,5-triol

There total 18 articles about (2R,3S,4R,5R,6R)-2-Hydroxymethyl-6-(4-methoxy-phenyl)-tetrahydro-pyran-3,4,5-triol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1384173-58-3
(4aR,6S,7S,8R,8aR)-2,2-di-tert-butyl-6-(4-methoxyphenyl)-8-[(triisopropylsilyl)oxy]hexahydropyrano[3,2-d][1,3,2]dioxasilin-7-ol

: 28538-11-6,109278-16-2,117772-56-2
(1S)-1,5-anhydro-1-(4-methoxyphenyl)-D-glucitol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 60 ℃; for 4h;
DOI:10.1016/j.tet.2012.05.035

Reference yield:

: 13139-86-1
4-methoxyphenyl magnesium bromide

: 572-10-1,4451-35-8,4451-36-9,14227-52-2,14227-87-3,14227-88-4,14257-40-0,17081-03-7,19186-60-8,57237-01-1,65982-17-4,65982-18-5,65982-19-6,66966-08-3,144299-57-0
2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl chloride

: 28538-11-6,109278-16-2,117772-56-2
(1S)-1-(4-methoxy-phenyl)-1,5-anhydro-D-mannitol

Guidance literature:: With diethyl ether; Behandeln nach Hydrolyse mit Acetanhydrid und Natriumacetat und Behandeln des Reaktionsprodukts mit Ammoniak in Methanol;