CHLOROTRIS(TRIPHENYLPHOSPHINE)COPPER(I)&

Base Information

• Chemical Name: CHLOROTRIS(TRIPHENYLPHOSPHINE)COPPER(I)&
• CAS No.: 15709-76-9
• Molecular Formula: C54H45 Cl Cu P3
• Molecular Weight: 885.872
• Mol file: 15709-76-9.mol

Synonyms:Copper,chlorotris(triphenylphosphine)- (7CI,8CI); Chlorotris(triphenylphosphine)copper

Chemical Property of CHLOROTRIS(TRIPHENYLPHOSPHINE)COPPER(I)&

Chemical Property:

• Melting Point: 175 °C (dec.)(lit.)
• PSA: 40.77000
• LogP: 10.21830

Purity/Quality:

99% ^*data from raw suppliers

Chlorotris(triphenylphosphine)copper(I) ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xn
• Statements: 20/21/22
• Safety Statements: 36/37

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of CHLOROTRIS(TRIPHENYLPHOSPHINE)COPPER(I)&

There total 17 articles about CHLOROTRIS(TRIPHENYLPHOSPHINE)COPPER(I)& which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

copper(II) choride dihydrate + triphenylphosphine (603-35-0) → tris(triphenylphosphino)copper(I) chloride (15709-76-9)

Guidance literature:

In methanol; stirring, pptn. (1 h); filtn., washing (MeOH), drying (vac.);

DOI:10.1002/zaac.19966220722

Reference yield: 82.0%

dichlorobis(triethylphosphine)palladium(II) (28425-04-9,15642-19-0,77027-39-5) + [Cu(CCSi(CH3)3)(P(C6H5)3)]4 + triphenylphosphine (603-35-0) → tris(triphenylphosphino)copper(I) chloride (15709-76-9) + trans-Pd(CCSiMe3)2(PEt3)2

Guidance literature:

In diethyl ether; Ar-atmosphere; stirring (room temp., 6 h); evapn., extg. (hexane), crystn. (-78°C); elem. anal.;

Reference yield: 80.0%

dichlorobis(triethylphosphine)palladium(II) (28425-04-9,15642-19-0,77027-39-5) + Cu2(CCCO2CH3)2(P(C6H5)3)3 (167114-10-5) + triphenylphosphine (603-35-0) → tris(triphenylphosphino)copper(I) chloride (15709-76-9) + trans-Pd(CCCOOMe)2(PEt3)2 (167114-16-1)

Guidance literature:

In toluene; N2 or Ar-atmosphere; stirring (4 h); filtering, washing (Et2O), evapn., recrystn. (hexane, -30°C); elem. anal.;

upstream raw materials:

copper(l) iodide

triphenylphosphine

dichlorobis(triethylphosphine)palladium(II)

catena-dichloro(3,6-dithiaoctane)copper(II)

Downstream raw materials:

Cu(P(C₆H₅)3)2(C₃H₅NS₂)Cl

CuCl(triphenylphosphane)₂(1-phenyl-1H-tetrazole-5(4H)-thione)

{Cu(P(C₆H₅)3)2(C₆H₅NC(O)CH₂NHC(S))Cl}

{Cu(P(C₆H₅)3)2(C₆H₅NHC(S)N(CH₂CH₂)2O)Cl}

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