(α)N-(2’-phenylacetyl)-aeg methyl ester

Base Information

Chemical Name:(α)N-(2’-phenylacetyl)-aeg methyl ester
CAS No.:1578249-75-8
Molecular Formula:C₁₈H₂₆N₂O₅
Molecular Weight:350.415
Hs Code.:

Synonyms:(α)N-(2’-phenylacetyl)-aeg methyl ester

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Chemical Property of (α)N-(2’-phenylacetyl)-aeg methyl ester

Chemical Property:

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Technology Process of (α)N-(2’-phenylacetyl)-aeg methyl ester

There total 2 articles about (α)N-(2’-phenylacetyl)-aeg methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 103-82-2
phenylacetic acid

: 128421-86-3
methyl N-(2-(tert-butyloxycarbonyl)aminoethyl)glycinate

: 1578249-75-8
(α)N-(2’-phenylacetyl)-aeg methyl ester

Guidance literature:: phenylacetic acid; With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; In N,N-dimethyl-formamide; Inert atmosphere; Cooling with ice;

methyl N-(2-(tert-butyloxycarbonyl)aminoethyl)glycinate; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1002/cplu.201300343

Reference yield:

: 57260-73-8
N-BOC-1,2-diaminoethane

: 1578249-75-8
(α)N-(2’-phenylacetyl)-aeg methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: KF celite / acetonitrile

2.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; benzotriazol-1-ol / N,N-dimethyl-formamide / Inert atmosphere; Cooling with ice

2.2: 20 °C

With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/cplu.201300343

Reference yield: 72.0%

: 1578249-75-8
(α)N-(2’-phenylacetyl)-aeg methyl ester

: 1578249-86-1
C₂₄H₂₈N₄O₄

Guidance literature:: (α)N-(2’-phenylacetyl)-aeg methyl ester; With chlorotriisopropylsilane; trifluoroacetic acid; In dichloromethane; for 1h; Cooling with ice;

In iso-butanol; at 110 ℃; Inert atmosphere; Acidic conditions;
DOI:10.1002/cplu.201300343