2-<3-phenylacetamido-4-thiochlorocarbonyl-(3R,4R)-azetidin-2-on-1-yl>-allyl acetate

Base Information

Chemical Name:2-<3-phenylacetamido-4-thiochlorocarbonyl-(3R,4R)-azetidin-2-on-1-yl>-allyl acetate
CAS No.:122691-78-5
Molecular Formula:C₁₇H₁₇ClN₂O₅S
Molecular Weight:396.851
Hs Code.:

Synonyms:2-<3-phenylacetamido-4-thiochlorocarbonyl-(3R,4R)-azetidin-2-on-1-yl>-allyl acetate

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Chemical Property of 2-<3-phenylacetamido-4-thiochlorocarbonyl-(3R,4R)-azetidin-2-on-1-yl>-allyl acetate

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Technology Process of 2-<3-phenylacetamido-4-thiochlorocarbonyl-(3R,4R)-azetidin-2-on-1-yl>-allyl acetate

There total 2 articles about 2-<3-phenylacetamido-4-thiochlorocarbonyl-(3R,4R)-azetidin-2-on-1-yl>-allyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 75-44-5
phosgene

: 124166-16-1
2-<3-phenylacetamido-4-thiol-(3R,4R)-azetidin-2-on-1-yl>-allyl acetate

: 122691-78-5
2-<3-phenylacetamido-4-thiochlorocarbonyl-(3R,4R)-azetidin-2-on-1-yl>-allyl acetate

Guidance literature:: With triethylamine; In dichloromethane; toluene; Ambient temperature;
DOI:10.1016/0223-5234(88)90100-6

Reference yield:

: 87996-79-0
2-<3-benzyl-6-oxo-2-thia-4,7-diaza-(1R,5R)-bicyclo-<3.2.0>-hept-3-en-7-yl>-allyl acetate

: 122691-78-5
2-<3-phenylacetamido-4-thiochlorocarbonyl-(3R,4R)-azetidin-2-on-1-yl>-allyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / 1.2 N aq HCl / dimethylformamide / 1 h / Ambient temperature

2: 68 percent / triethylamine / toluene; CH₂Cl₂ / Ambient temperature

With hydrogenchloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/0223-5234(88)90100-6

Reference yield:

: 122691-78-5
2-<3-phenylacetamido-4-thiochlorocarbonyl-(3R,4R)-azetidin-2-on-1-yl>-allyl acetate

: 122692-08-4
2-<3-phenylacetamido-4-(N-diethyl)thiocarbamate-(3R,4R)-azetidin-2-on-1-yl>acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / 2 h / 20 °C

2: 64 percent / Pd⁰-triphenylphosphine complex, 2-ethylhexanoic acid / 20 °C

With palladium-triphenylphosphine; 2-Ethylhexanoic acid; In dichloromethane;
DOI:10.1016/0223-5234(88)90100-6