1-(3-azido-2,3-dideoxy-5-O-p-monomethoxytrityl-β-D-erythro-pentofuranosyl)-lumazine

Base Information

Chemical Name:1-(3-azido-2,3-dideoxy-5-O-p-monomethoxytrityl-β-D-erythro-pentofuranosyl)-lumazine
CAS No.:159228-17-8
Molecular Formula:C₃₁H₂₇N₇O₅
Molecular Weight:577.599
Hs Code.:

Synonyms:1-(3-azido-2,3-dideoxy-5-O-p-monomethoxytrityl-β-D-erythro-pentofuranosyl)-lumazine

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Chemical Property of 1-(3-azido-2,3-dideoxy-5-O-p-monomethoxytrityl-β-D-erythro-pentofuranosyl)-lumazine

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Technology Process of 1-(3-azido-2,3-dideoxy-5-O-p-monomethoxytrityl-β-D-erythro-pentofuranosyl)-lumazine

There total 5 articles about 1-(3-azido-2,3-dideoxy-5-O-p-monomethoxytrityl-β-D-erythro-pentofuranosyl)-lumazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 159228-20-3
1-(2-deoxy-3-O-mesyl-5-O-p-monomethoxytrityl-β-D-threo-pentofuranosyl)-lumazine

: 159228-17-8
1-(3-azido-2,3-dideoxy-5-O-p-monomethoxytrityl-β-D-erythro-pentofuranosyl)-lumazine

Guidance literature:: With lithium azide; In N,N-dimethyl-formamide; at 80 ℃; for 4h;
DOI:10.1080/15257779408013278

Reference yield:

: 71470-93-4
1-(2-deoxy-5-O-p-monomethoxytrityl-β-D-erythro-pentofuranosyl)-lumazine

: 159228-17-8
1-(3-azido-2,3-dideoxy-5-O-p-monomethoxytrityl-β-D-erythro-pentofuranosyl)-lumazine

Guidance literature:: Multi-step reaction with 5 steps

1: 91 percent / pyridine / 2 h / 0 °C

2: 84 percent / DBU / CH₂Cl₂ / 1 h / Heating

3: 85 percent / aq. sodium hydroxide / ethanol / 1 h / Heating

4: 86 percent / pyridine / 2 h / 0 °C

5: 75 percent / lithium azide / dimethylformamide / 4 h / 80 °C

With sodium hydroxide; lithium azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In pyridine; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1080/15257779408013278

Reference yield:

: 2,3'-anhydro-1-(2-deoxy-5-O-p-monomethoxytrityl-β-D-threo-pentofuranosyl)-lumazine

: 159228-17-8
1-(3-azido-2,3-dideoxy-5-O-p-monomethoxytrityl-β-D-erythro-pentofuranosyl)-lumazine

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / aq. sodium hydroxide / ethanol / 1 h / Heating

2: 86 percent / pyridine / 2 h / 0 °C

3: 75 percent / lithium azide / dimethylformamide / 4 h / 80 °C

With sodium hydroxide; lithium azide; In pyridine; ethanol; N,N-dimethyl-formamide;
DOI:10.1080/15257779408013278