1-(2-deoxy-3-O-mesyl-5-O-p-monomethoxytrityl-β-D-erythro-pentofuranosyl)-lumazine

Base Information

Chemical Name:1-(2-deoxy-3-O-mesyl-5-O-p-monomethoxytrityl-β-D-erythro-pentofuranosyl)-lumazine
CAS No.:159228-16-7
Molecular Formula:C₃₂H₃₀N₄O₈S
Molecular Weight:630.678
Hs Code.:

Synonyms:1-(2-deoxy-3-O-mesyl-5-O-p-monomethoxytrityl-β-D-erythro-pentofuranosyl)-lumazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2-deoxy-3-O-mesyl-5-O-p-monomethoxytrityl-β-D-erythro-pentofuranosyl)-lumazine

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Technology Process of 1-(2-deoxy-3-O-mesyl-5-O-p-monomethoxytrityl-β-D-erythro-pentofuranosyl)-lumazine

There total 1 articles about 1-(2-deoxy-3-O-mesyl-5-O-p-monomethoxytrityl-β-D-erythro-pentofuranosyl)-lumazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 71470-93-4
1-(2-deoxy-5-O-p-monomethoxytrityl-β-D-erythro-pentofuranosyl)-lumazine

: 124-63-0
methanesulfonyl chloride

: 159228-16-7
1-(2-deoxy-3-O-mesyl-5-O-p-monomethoxytrityl-β-D-erythro-pentofuranosyl)-lumazine

Guidance literature:: In pyridine; at 0 ℃; for 2h;
DOI:10.1080/15257779408013278

Reference yield: 84.0%

: 159228-16-7
1-(2-deoxy-3-O-mesyl-5-O-p-monomethoxytrityl-β-D-erythro-pentofuranosyl)-lumazine

: 2,3'-anhydro-1-(2-deoxy-5-O-p-monomethoxytrityl-β-D-threo-pentofuranosyl)-lumazine

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; for 1h; Heating;
DOI:10.1080/15257779408013278

Reference yield:

: 159228-16-7
1-(2-deoxy-3-O-mesyl-5-O-p-monomethoxytrityl-β-D-erythro-pentofuranosyl)-lumazine

: 159228-17-8
1-(3-azido-2,3-dideoxy-5-O-p-monomethoxytrityl-β-D-erythro-pentofuranosyl)-lumazine

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / DBU / CH₂Cl₂ / 1 h / Heating

2: 85 percent / aq. sodium hydroxide / ethanol / 1 h / Heating

3: 86 percent / pyridine / 2 h / 0 °C

4: 75 percent / lithium azide / dimethylformamide / 4 h / 80 °C

With sodium hydroxide; lithium azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In pyridine; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1080/15257779408013278