7-(2,4-Dichloro-phenyl)-2-methyl-3-(2H-tetrazol-5-ylmethyl)-2H-indazole

Base Information

• Chemical Name: 7-(2,4-Dichloro-phenyl)-2-methyl-3-(2H-tetrazol-5-ylmethyl)-2H-indazole
• CAS No.: 952236-28-1
• Molecular Formula: C₁₆H₁₂Cl₂N₆
• Molecular Weight: 359.217

Synonyms:7-(2,4-Dichloro-phenyl)-2-methyl-3-(2H-tetrazol-5-ylmethyl)-2H-indazole

Chemical Property of 7-(2,4-Dichloro-phenyl)-2-methyl-3-(2H-tetrazol-5-ylmethyl)-2H-indazole

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Technology Process of 7-(2,4-Dichloro-phenyl)-2-methyl-3-(2H-tetrazol-5-ylmethyl)-2H-indazole

There total 1 articles about 7-(2,4-Dichloro-phenyl)-2-methyl-3-(2H-tetrazol-5-ylmethyl)-2H-indazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

[7-(2,4-Dichloro-phenyl)-2-methyl-2H-indazol-3-yl]-acetonitrile (845750-73-4) → 7-(2,4-Dichloro-phenyl)-2-methyl-3-(2H-tetrazol-5-ylmethyl)-2H-indazole (952236-28-1)

Guidance literature:

With azido tributyltin (IV); In toluene; at 110 ℃;

Reference yield: 58.0%

7-(2,4-Dichloro-phenyl)-2-methyl-3-(2H-tetrazol-5-ylmethyl)-2H-indazole (952236-28-1) + chloro-methylsulfanyl-methane (2373-51-5) → 7-(2,4-Dichloro-phenyl)-2-methyl-3-(2-methylsulfanylmethyl-2H-tetrazol-5-ylmethyl)-2H-indazole (952236-38-3) + 7-(2,4-dichloro-phenyl)-2-methyl-3-(1-methylsulfanylmethyl-1H-tetrazol-5-ylmethyl)-2H-indazole (952236-39-4)

Guidance literature:

In chloro-methylsulfanyl-methane; at 100 ℃; for 2.5h;

Reference yield: 25.0%

7-(2,4-Dichloro-phenyl)-2-methyl-3-(2H-tetrazol-5-ylmethyl)-2H-indazole (952236-28-1) → [7-(2,4-Dichloro-phenyl)-2-methyl-2H-indazol-3-yl]-(1-methyl-1H-tetrazol-5-yl)-methanol + 7-(2,4-dichloro-phenyl)-2-methyl-3-(2-methyl-2H-tetrazol-5-ylmethyl)-2H-indazole

Guidance literature:

With potassium carbonate; methyl iodide; In N,N-dimethyl-formamide; at 20 ℃;

upstream raw materials:

[7-(2,4-Dichloro-phenyl)-2-methyl-2H-indazol-3-yl]-acetonitrile

Downstream raw materials:

7-(2,4-Dichloro-phenyl)-2-methyl-3-(2-methylsulfanylmethyl-2H-tetrazol-5-ylmethyl)-2H-indazole

7-(2,4-dichloro-phenyl)-2-methyl-3-(1-methylsulfanylmethyl-1H-tetrazol-5-ylmethyl)-2H-indazole

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