tetrabutylammonium {tris[3,5-bis(trifluoromethyl)phenyl]{4-[(dibenzo[d,f][1,3,2]dioxaphosphepine-6-yloxy)methyl]-2,3,5,6-tetrafluorophenyl}borate}

Base Information

Chemical Name:tetrabutylammonium {tris[3,5-bis(trifluoromethyl)phenyl]{4-[(dibenzo[d,f][1,3,2]dioxaphosphepine-6-yloxy)methyl]-2,3,5,6-tetrafluorophenyl}borate}
CAS No.:1453219-77-6
Molecular Formula:C₁₆H₃₆N*C₄₃H₁₉BF₂₂O₃P
Molecular Weight:1285.84
Hs Code.:

tetrabutylammonium {tris[3,5-bis(trifluoromethyl)phenyl]{4-[(dibenzo[d,f][1,3,2]dioxaphosphepine-6-yloxy)methyl]-2,3,5,6-tetrafluorophenyl}borate}

Synonyms:tetrabutylammonium {tris[3,5-bis(trifluoromethyl)phenyl]{4-[(dibenzo[d,f][1,3,2]dioxaphosphepine-6-yloxy)methyl]-2,3,5,6-tetrafluorophenyl}borate}

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Chemical Property of tetrabutylammonium {tris[3,5-bis(trifluoromethyl)phenyl]{4-[(dibenzo[d,f][1,3,2]dioxaphosphepine-6-yloxy)methyl]-2,3,5,6-tetrafluorophenyl}borate}

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Technology Process of tetrabutylammonium {tris[3,5-bis(trifluoromethyl)phenyl]{4-[(dibenzo[d,f][1,3,2]dioxaphosphepine-6-yloxy)methyl]-2,3,5,6-tetrafluorophenyl}borate}

There total 2 articles about tetrabutylammonium {tris[3,5-bis(trifluoromethyl)phenyl]{4-[(dibenzo[d,f][1,3,2]dioxaphosphepine-6-yloxy)methyl]-2,3,5,6-tetrafluorophenyl}borate} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1013095-35-6
tetrabutylammonium (2,3,5,6-tetrafluoro-4-hydroxymethylphenyl)tris[3,5-bis(trifluoromethyl)phenyl]borate

: 16611-68-0
6-chloro-dibenzo[d,f][1,3,2]-dioxaphosphepin

: 1453219-77-6
tetrabutylammonium {tris[3,5-bis(trifluoromethyl)phenyl]{4-[(dibenzo[d,f][1,3,2]dioxaphosphepine-6-yloxy)methyl]-2,3,5,6-tetrafluorophenyl}borate}

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 19h; Inert atmosphere; Schlenk technique;
DOI:10.1002/chem.201202408

Reference yield:

: 1806-29-7
2,2'-dihydroxybiphenyl

: 1453219-77-6
tetrabutylammonium {tris[3,5-bis(trifluoromethyl)phenyl]{4-[(dibenzo[d,f][1,3,2]dioxaphosphepine-6-yloxy)methyl]-2,3,5,6-tetrafluorophenyl}borate}

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; phosphorus trichloride / tetrahydrofuran / 2.58 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

2: triethylamine / tetrahydrofuran / 19 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

With triethylamine; phosphorus trichloride; In tetrahydrofuran;
DOI:10.1002/chem.201202408