(S)-2-{(S)-2-[(S)-2-benzyloxycarbonylamino-3-(4-hydroxyphenyl)propionylamino]-4-methylpentanoylamino}-6-hydroxyhexanoic acid methyl ester

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Chemical Name:(S)-2-{(S)-2-[(S)-2-benzyloxycarbonylamino-3-(4-hydroxyphenyl)propionylamino]-4-methylpentanoylamino}-6-hydroxyhexanoic acid methyl ester
CAS No.:1020257-88-8
Molecular Formula:C₃₀H₄₁N₃O₈
Molecular Weight:571.671
Hs Code.:

Synonyms:(S)-2-{(S)-2-[(S)-2-benzyloxycarbonylamino-3-(4-hydroxyphenyl)propionylamino]-4-methylpentanoylamino}-6-hydroxyhexanoic acid methyl ester

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Chemical Property of (S)-2-{(S)-2-[(S)-2-benzyloxycarbonylamino-3-(4-hydroxyphenyl)propionylamino]-4-methylpentanoylamino}-6-hydroxyhexanoic acid methyl ester

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Technology Process of (S)-2-{(S)-2-[(S)-2-benzyloxycarbonylamino-3-(4-hydroxyphenyl)propionylamino]-4-methylpentanoylamino}-6-hydroxyhexanoic acid methyl ester

There total 2 articles about (S)-2-{(S)-2-[(S)-2-benzyloxycarbonylamino-3-(4-hydroxyphenyl)propionylamino]-4-methylpentanoylamino}-6-hydroxyhexanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 35971-70-1
(S)-2-[(S)-2-benzyloxycarbonylamino-3-(4-hydroxy-phenyl)-propionylamino]-4-methyl pentanoic acid

: 121895-18-9
(S)-2-amino-6-hydroxyhexanoic acid methyl ester hydrochloride

: 1020257-88-8
(S)-2-{(S)-2-[(S)-2-benzyloxycarbonylamino-3-(4-hydroxyphenyl)propionylamino]-4-methylpentanoylamino}-6-hydroxyhexanoic acid methyl ester

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 48h; Inert atmosphere;
DOI:10.1071/CH09101

Reference yield:

: 35971-70-1
(S)-2-[(S)-2-benzyloxycarbonylamino-3-(4-hydroxy-phenyl)-propionylamino]-4-methyl pentanoic acid

: 167090-40-6,781578-64-1
(S)-2-amino-6-hydroxy-hexanoic acid methyl ester

: 1020257-88-8
(S)-2-{(S)-2-[(S)-2-benzyloxycarbonylamino-3-(4-hydroxyphenyl)propionylamino]-4-methylpentanoylamino}-6-hydroxyhexanoic acid methyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield: 75.0%

: 1020257-88-8
(S)-2-{(S)-2-[(S)-2-benzyloxycarbonylamino-3-(4-hydroxyphenyl)propionylamino]-4-methylpentanoylamino}-6-hydroxyhexanoic acid methyl ester

: 1198577-42-2
(S)-2-{(S)-2-[(S)-2-benzyloxycarbonylamino-3-(4-hydroxyphenyl)propionylamino]-4-methylpentanoylamino}-6-iodohexanoic acid methyl ester

Guidance literature:: With tetra-(n-butyl)ammonium iodide; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1071/CH09101