1-(2-METHOXYPHENYL)-2-PROPANOL 98

Base Information

• Chemical Name: 1-(2-METHOXYPHENYL)-2-PROPANOL 98
• CAS No.: 15541-26-1
• Molecular Formula: C10H14 O2
• Molecular Weight: 166.22
• Hs Code.: 2909499000
• Mol file: 15541-26-1.mol

Synonyms:Phenethylalcohol, o-methoxy-a-methyl- (8CI)

Chemical Property of 1-(2-METHOXYPHENYL)-2-PROPANOL 98

Chemical Property:

• Refractive Index: n20/D 1.529(lit.)
• Flash Point: >230 °F
• PSA: 29.46000
• Density: 1.035 g/mL at 25 °C(lit.)
• LogP: 1.61850
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

98%min ^*data from raw suppliers

1-(2-Methoxyphenyl)propan-2-ol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(2-METHOXYPHENYL)-2-PROPANOL 98

There total 8 articles about 1-(2-METHOXYPHENYL)-2-PROPANOL 98 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

1-(2-methoxyphenyl)propan-2-one (5211-62-1) → 1-(2-methoxyphenyl)-2-propanol (15541-26-1)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/ol101336y

Reference yield: 79.0%

2-bromoanisole (578-57-4) + methyloxirane (75-56-9,16033-71-9) → 1-(2-methoxyphenyl)-2-propanol (15541-26-1)

Guidance literature:

2-bromoanisole; With n-butyllithium; In tetrahydrofuran; hexane; at -70 ℃;

methyloxirane; In tetrahydrofuran; hexane; at -50 - 20 ℃;

DOI:10.1016/j.tetasy.2005.12.025

Reference yield: 57.0%

methoxybenzene (100-66-3) + methyloxirane (75-56-9,16033-71-9) → 1-(2-methoxyphenyl)-2-propanol (15541-26-1)

Guidance literature:

methoxybenzene; With lithium (tetra)butylmagnesate; In tetrahydrofuran; hexane; Reflux; Inert atmosphere;

methyloxirane; In tetrahydrofuran; hexane; at 20 ℃; Inert atmosphere;

DOI:10.1039/c0cc01731k

upstream raw materials:

1-(2-methoxyphenyl)propan-2-one

2-allylanisole

2-bromoanisole

methyloxirane

Downstream raw materials:

1-(2-methoxyphenyl)propan-2-yl acetate