Technology Process of C16H20O
There total 4 articles about C16H20O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
methyl magnesium iodide; (Z)-3-phenylnon-2-en-4-ynal;
In
diethyl ether;
at -78 - 20 ℃;
With
hydrogenchloride; water;
In
diethyl ether;
at -20 ℃;
DOI:10.1021/ol102989q
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: acetic acid; sodium iodide / 3 h / 115 °C
2.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 0.17 h / 20 °C / Inert atmosphere
2.2: 3 h / 20 °C / Inert atmosphere
3.1: diisobutylaluminium hydride / hexane; dichloromethane / -78 °C / Inert atmosphere
4.1: diethyl ether / -78 - 20 °C
4.2: -20 °C
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisobutylaluminium hydride; acetic acid; triethylamine; sodium iodide;
In
diethyl ether; hexane; dichloromethane;
DOI:10.1021/ol102989q
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 0.17 h / 20 °C / Inert atmosphere
1.2: 3 h / 20 °C / Inert atmosphere
2.1: diisobutylaluminium hydride / hexane; dichloromethane / -78 °C / Inert atmosphere
3.1: diethyl ether / -78 - 20 °C
3.2: -20 °C
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisobutylaluminium hydride; triethylamine;
In
diethyl ether; hexane; dichloromethane;
DOI:10.1021/ol102989q
