C₄₆H₄₆O₉Si

Base Information

• Chemical Name: C₄₆H₄₆O₉Si
• CAS No.: 1228755-40-5
• Molecular Formula: C₄₆H₄₆O₉Si
• Molecular Weight: 770.951
• Mol file: 1228755-40-5.mol

Synonyms:C₄₆H₄₆O₉Si

Chemical Property of C₄₆H₄₆O₉Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₆H₄₆O₉Si

There total 3 articles about C₄₆H₄₆O₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Acetic acid (2R,3R,4S,5R,6R)-3,5-diacetoxy-2-acetoxymethyl-6-allyloxy-tetrahydro-pyran-4-yl ester (10343-15-4,39698-55-0,54400-76-9,78730-32-2,119111-31-8,119111-32-9) → C46H46O9Si (1228755-40-5)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium methylate / methanol / 1 h

2: pyridine / 20 °C / Cooling with ice

3: pyridine / 20 °C / Cooling with ice

With pyridine; sodium methylate; In methanol;

DOI:10.1002/chem.201302572

Reference yield:

C25H34O6Si + benzoyl chloride (98-88-4) → C46H46O9Si (1228755-40-5)

Guidance literature:

With pyridine; at 20 ℃; Cooling with ice;

DOI:10.1002/chem.201302572

Reference yield:

allyl β-D-glucopyranoside (2595-07-5,7464-56-4,34384-79-7,41308-76-3,48149-72-0,48149-74-2,85249-43-0,119479-69-5,821794-45-0) → C46H46O9Si (1228755-40-5)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / 20 °C / Cooling with ice

2: pyridine / 20 °C / Cooling with ice

With pyridine;

DOI:10.1002/chem.201302572

upstream raw materials:

benzoyl chloride

Acetic acid (2R,3R,4S,5R,6R)-3,5-diacetoxy-2-acetoxymethyl-6-allyloxy-tetrahydro-pyran-4-yl ester

allyl β-D-glucopyranoside

Downstream raw materials:

2,3,4-tri-O-benzoyl-1-deoxy-1-(2,2,2-trichloro-1-iminoethoxy)-α-D-glucopyranuronate, methyl ester

allyl 2,3,4-tri-O-benzoyl-β-D-glucopyranoside