(1R,2R)-trans-cyclohexanediol mono

Base Information

Chemical Name:(1R,2R)-trans-cyclohexanediol mono
CAS No.:135570-20-6
Molecular Formula:C₁₅H₂₁NO₃
Molecular Weight:263.337
Hs Code.:

(1R,2R)-trans-cyclohexanediol mono<p-(dimethylamino)benzoate>

Synonyms:(1R,2R)-trans-cyclohexanediol mono

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Chemical Property of (1R,2R)-trans-cyclohexanediol mono

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Technology Process of (1R,2R)-trans-cyclohexanediol mono

There total 2 articles about (1R,2R)-trans-cyclohexanediol mono which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-24-7
acetic anhydride

: (trans)-4-dimethylaminobenzoic acid 2-hydroxycyclohexyl ester

: C₁₅H₂₁NO₃

: 1174192-86-9
C₁₇H₂₃NO₄

: C₁₇H₂₃NO₄

: 135570-20-6
(1R,2R)-trans-cyclohexanediol mono

Guidance literature:: With triethylamine; In toluene; at 20 ℃; for 16h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1002/chem.200900532

Reference yield:

: 1072-86-2,1460-57-7,1792-81-0,54383-22-1,57794-08-8,931-17-9
(1R,2R)-trans-1,2-cyclohexanediol

: 619-84-1
p-N,N-dimethylaminobenzoic acid

: 135570-20-6
(1R,2R)-trans-cyclohexanediol mono

Guidance literature:: With 4 A molecular sieve; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1,1'-carbonyldiimidazole; Yield given. Multistep reaction; 1) DMSO, 20-30 min, 40 deg C, 2) 40 - 50 deg C, 10 - 15 h;
DOI:10.1021/jo00021a013