benzyl-5-(3-azido-propyl)-3-hydroxy-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one ethylene glycol acetal

Base Information

• Chemical Name: benzyl-5-(3-azido-propyl)-3-hydroxy-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one ethylene glycol acetal
• CAS No.: 1013941-05-3
• Molecular Formula: C₃₀H₃₇N₃O₃
• Molecular Weight: 487.642

Synonyms:benzyl-5-(3-azido-propyl)-3-hydroxy-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one ethylene glycol acetal

Chemical Property of benzyl-5-(3-azido-propyl)-3-hydroxy-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one ethylene glycol acetal

Chemical Property:

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Technology Process of benzyl-5-(3-azido-propyl)-3-hydroxy-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one ethylene glycol acetal

There total 1 articles about benzyl-5-(3-azido-propyl)-3-hydroxy-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one ethylene glycol acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

15-(3-azido-propyl)-3-benzyloxy-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one (1013940-37-8) + ethylene glycol (107-21-1) → benzyl-5-(3-azido-propyl)-3-hydroxy-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one ethylene glycol acetal (1013941-05-3)

Guidance literature:

With toluene-4-sulfonic acid; orthoformic acid triethyl ester; at 40 ℃;

Reference yield: 83.0%

benzyl-5-(3-azido-propyl)-3-hydroxy-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one ethylene glycol acetal (1013941-05-3) + 4-n-methylphenylacetylene (766-97-2) → 3-benzyloxy-15-[3-(4-p-tolyl-[1,2,3]triazol-1-yl)-propyl]-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one ethylene glycol acetal (1013941-13-3)

Guidance literature:

With copper(II) sulfate; sodium L-ascorbate; In ethanol; water; at 120 ℃; for 0.166667h; Microwave irradiation;

Reference yield: 78.0%

benzyl-5-(3-azido-propyl)-3-hydroxy-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one ethylene glycol acetal (1013941-05-3) + 5-methylhex-1-yne (2203-80-7) → 3-benzyloxy-15-[3-(4-isopentyl-[1,2,3]triazol-1-yl)-propyl]-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one ethylene glycol acetal (1013941-21-3)

Guidance literature:

With copper(II) sulfate; sodium L-ascorbate; In ethanol; water; at 120 ℃; for 0.166667h; Microwave irradiation;

upstream raw materials:

15-(3-azido-propyl)-3-benzyloxy-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one

ethylene glycol

Downstream raw materials:

3-benzyloxy-15-[3-(4-m-hydroxyphenyl-[1,2,3]triazol-1-yl)-propyl]-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one ethylene glycol acetal

3-benzyloxy-15-[3-(4-p-tolyl-[1,2,3]triazol-1-yl)-propyl]-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one ethylene glycol acetal

3-benzyloxy-15-[3-(4-isobutyl-[1,2,3]triazol-1-yl)-propyl]-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one ethylene glycol acetal

3-benzyloxy-15-[3-(4-(2-phenylethane)-[1,2,3]triazol-1-yl)-propyl]-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one ethylene glycol acetal

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