9-Phenanthrenemethanamine

Base Information

• Chemical Name: 9-Phenanthrenemethanamine
• CAS No.: 15398-91-1
• Molecular Formula: C₁₅H₁₃N
• Molecular Weight: 207.275
• Hs Code.: 2921499090
• DSSTox Substance ID: DTXSID60331241
• Nikkaji Number: J1.145.969B
• Wikidata: Q82096261
• Mol file: 15398-91-1.mol

Synonyms:9-Phenanthrenemethanamine;15398-91-1;C-Phenanthren-9-yl-methylamine;phenanthren-9-ylmethanamine;SCHEMBL8517693;DTXSID60331241;1-(PHENANTHREN-9-YL)METHANAMINE

Chemical Property of 9-Phenanthrenemethanamine

Chemical Property:

• PSA: 26.02000
• LogP: 4.15200
• XLogP3: 3.3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 207.104799419
• Heavy Atom Count: 16
• Complexity: 238

Purity/Quality:

99% ^*data from raw suppliers

C-Phenanthren-9-yl-methylamine 95 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)C=C(C3=CC=CC=C23)CN

Technology Process of 9-Phenanthrenemethanamine

There total 10 articles about 9-Phenanthrenemethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 9-phenanthrylmethylamine (15398-91-1)

Guidance literature:

With acetic acid; platinum; Hydrogenation;

DOI:10.1080/09585180122116

Reference yield:

9-hydroxymethylphenanthrene (4707-72-6) → 9-phenanthrylmethylamine (15398-91-1)

Guidance literature:

Multi-step reaction with 2 steps

1: concentrated aqueous HCl / 100 °C

2: ammonia / fluessiges Ammoniak

With hydrogenchloride; ammonia;

Reference yield:

Phenanthrene-9-carboxaldehyde (4707-71-5) → 9-phenanthrylmethylamine (15398-91-1)

Guidance literature:

Multi-step reaction with 4 steps

1: sodium tetrahydroborate

2: carbon tetrabromide; triphenylphosphine

3: sodium azide

4: triphenylphosphine

With sodium tetrahydroborate; sodium azide; carbon tetrabromide; triphenylphosphine;

DOI:10.1021/ma302344x

upstream raw materials:

9-(chloromethyl)phenanthrene

phenanthrene-9-carboxamide

ammonia

9-hydroxymethylphenanthrene