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Technology Process of F2BN(NC4H(C6H5)C6H4OOCC6H4(C6H5)3C20H8N4Zn)(NC4H(C6H5)C6H4OH)

F2BN(NC4H(C6H5)C6H4OOCC6H4(C6H5)3C20H8N4Zn)(NC4H(C6H5)C6H4OH)

Base Information
  • Chemical Name:F2BN(NC4H(C6H5)C6H4OOCC6H4(C6H5)3C20H8N4Zn)(NC4H(C6H5)C6H4OH)
  • CAS No.:1352229-34-5
  • Molecular Formula:C77H48BF2N7O3Zn
  • Molecular Weight:1233.47
  • Hs Code.:
F<sub>2</sub>BN(NC<sub>4</sub>H(C<sub>6</sub>H<sub>5</sub>)C<sub>6</sub>H<sub>4</sub>OOCC<sub>6</sub>H<sub>4</sub>(C<sub>6</sub>H<sub>5</sub>)3C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>Zn)(NC<sub>4</sub>H(C<sub>6</sub>H<sub>5</sub>)C<sub>6</sub>H<sub>4</sub>OH)

Synonyms:F2BN(NC4H(C6H5)C6H4OOCC6H4(C6H5)3C20H8N4Zn)(NC4H(C6H5)C6H4OH)

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Chemical Property of F2BN(NC4H(C6H5)C6H4OOCC6H4(C6H5)3C20H8N4Zn)(NC4H(C6H5)C6H4OH)
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Technology Process of F2BN(NC4H(C6H5)C6H4OOCC6H4(C6H5)3C20H8N4Zn)(NC4H(C6H5)C6H4OH)

There total 2 articles about F2BN(NC4H(C6H5)C6H4OOCC6H4(C6H5)3C20H8N4Zn)(NC4H(C6H5)C6H4OH) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

C<sub>77</sub>H<sub>50</sub>BF<sub>2</sub>N<sub>7</sub>O<sub>3</sub>

C77H50BF2N7O3

F<sub>2</sub>BN(NC<sub>4</sub>H(C<sub>6</sub>H<sub>5</sub>)C<sub>6</sub>H<sub>4</sub>OOCC<sub>6</sub>H<sub>4</sub>(C<sub>6</sub>H<sub>5</sub>)3C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>Zn)(NC<sub>4</sub>H(C<sub>6</sub>H<sub>5</sub>)C<sub>6</sub>H<sub>4</sub>OH)
1352229-34-5

F2BN(NC4H(C6H5)C6H4OOCC6H4(C6H5)3C20H8N4Zn)(NC4H(C6H5)C6H4OH)

Guidance literature:
With zinc diacetate; In methanol; chloroform; for 12h;
DOI:10.1021/ja209718g

Reference yield: 85.0%

F<sub>2</sub>BN(NC<sub>4</sub>H(C<sub>6</sub>H<sub>5</sub>)C<sub>6</sub>H<sub>4</sub>OOCC<sub>6</sub>H<sub>4</sub>(C<sub>6</sub>H<sub>5</sub>)3C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>H<sub>2</sub>)(NC<sub>4</sub>H(C<sub>6</sub>H<sub>5</sub>)C<sub>6</sub>H<sub>4</sub>OH)

F2BN(NC4H(C6H5)C6H4OOCC6H4(C6H5)3C20H8N4H2)(NC4H(C6H5)C6H4OH)

zinc diacetate
557-34-6

zinc diacetate

F<sub>2</sub>BN(NC<sub>4</sub>H(C<sub>6</sub>H<sub>5</sub>)C<sub>6</sub>H<sub>4</sub>OOCC<sub>6</sub>H<sub>4</sub>(C<sub>6</sub>H<sub>5</sub>)3C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>Zn)(NC<sub>4</sub>H(C<sub>6</sub>H<sub>5</sub>)C<sub>6</sub>H<sub>4</sub>OH)
1352229-34-5

F2BN(NC4H(C6H5)C6H4OOCC6H4(C6H5)3C20H8N4Zn)(NC4H(C6H5)C6H4OH)

Guidance literature:
In methanol; chloroform; satd. soln. of Zn(OAc)2 in MeOH added to soln. of azaBODIPY-porphyrin deriv. in CHCl3, mixt. stirred for 12 h; mixt. washed with water, org. layer sepd., dried over Na2SO4, filtrate evapd., chromy. (silica gel, CHCl3); MS;
DOI:10.1021/ja209718g
upstream raw materials:

zinc diacetate

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