(4E,8E,2R,3S,2'S)-N-2'-acetoxyhexadecanoyl-1-O-benzoyl-9-methyl-4,8-sphingadienine

Base Information

Chemical Name:(4E,8E,2R,3S,2'S)-N-2'-acetoxyhexadecanoyl-1-O-benzoyl-9-methyl-4,8-sphingadienine
CAS No.:105369-19-5
Molecular Formula:C₄₄H₇₃NO₆
Molecular Weight:712.067
Hs Code.:

Synonyms:(4E,8E,2R,3S,2'S)-N-2'-acetoxyhexadecanoyl-1-O-benzoyl-9-methyl-4,8-sphingadienine

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Chemical Property of (4E,8E,2R,3S,2'S)-N-2'-acetoxyhexadecanoyl-1-O-benzoyl-9-methyl-4,8-sphingadienine

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Technology Process of (4E,8E,2R,3S,2'S)-N-2'-acetoxyhexadecanoyl-1-O-benzoyl-9-methyl-4,8-sphingadienine

There total 10 articles about (4E,8E,2R,3S,2'S)-N-2'-acetoxyhexadecanoyl-1-O-benzoyl-9-methyl-4,8-sphingadienine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 88195-83-9
p-nitrophenyl (S)-2-acetoxyhexadecanoate

: Benzoic acid (4E,8E)-(2R,3S)-2-amino-3-hydroxy-9-methyl-octadeca-4,8-dienyl ester; hydrochloride

: 105369-19-5
(4E,8E,2R,3S,2'S)-N-2'-acetoxyhexadecanoyl-1-O-benzoyl-9-methyl-4,8-sphingadienine

Guidance literature:: In pyridine; at 45 - 50 ℃; for 24h; Yield given;

Reference yield:

: 88195-83-9
p-nitrophenyl (S)-2-acetoxyhexadecanoate

: 105369-19-5
(4E,8E,2R,3S,2'S)-N-2'-acetoxyhexadecanoyl-1-O-benzoyl-9-methyl-4,8-sphingadienine

Guidance literature:: In pyridine; hexane;

Reference yield:

: 78330-57-1
(2S)-2-hydroxyhexadecanoic acid methyl ester

: 105369-19-5
(4E,8E,2R,3S,2'S)-N-2'-acetoxyhexadecanoyl-1-O-benzoyl-9-methyl-4,8-sphingadienine

Guidance literature:: Multi-step reaction with 4 steps

1: 88.3 percent / KOH / ethanol / 0.33 h / 70 °C

2: 95 percent / pyridine / 1.) rt, 1 h; 2.) ice-cooling, 10 min

3: 94 percent / pyridine / 18 h / Ambient temperature

4: pyridine / 24 h / 45 - 50 °C

With potassium hydroxide; In pyridine; ethanol;