(2S,3R)-2-benzyloxy-3-hydrazononane

Base Information

Chemical Name:(2S,3R)-2-benzyloxy-3-hydrazononane
CAS No.:93367-14-7
Molecular Formula:C₁₆H₂₅N₃O
Molecular Weight:275.394
Hs Code.:

Synonyms:(2S,3R)-2-benzyloxy-3-hydrazononane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R)-2-benzyloxy-3-hydrazononane

Chemical Property:

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Technology Process of (2S,3R)-2-benzyloxy-3-hydrazononane

There total 10 articles about (2S,3R)-2-benzyloxy-3-hydrazononane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 81408-36-8
(2S,3S)-2-O-benzyl-2,3-nonanediol

: 93367-14-7
(2S,3R)-2-benzyloxy-3-hydrazononane

Guidance literature:: With tris-(2-chloro-ethyl)-amine; triphenylphosphine; diethylazodicarboxylate; In benzene;
DOI:10.1016/S0040-4039(00)83984-2

Reference yield:

: 104079-62-1,104113-19-1
(S)-1-((S)-6-Ethyl-6-phenylsulfanyl-tetrahydro-pyran-2-yl)-ethanol

: 93367-14-7
(2S,3R)-2-benzyloxy-3-hydrazononane

Guidance literature:: Multi-step reaction with 3 steps

1: 2.) AlCl₃ / 1.) protection with benzyl ether 2.) CH₂Cl₂, 0 gradC, 1.5 h.

2: 72 percent / Reney-nickel / ethanol / 0.5 h / 20 °C

3: 85 percent / HN₃, Ph₃P, diethyl azodicarboxylate / benzene

With aluminium trichloride; tris-(2-chloro-ethyl)-amine; triphenylphosphine; diethylazodicarboxylate; Reney-nickel; In ethanol; benzene;
DOI:10.1016/S0040-4039(00)83984-2

Reference yield:

: 104101-25-9
Methanesulfonic acid (1S,5S,7S)-5-ethyl-6,8-dioxa-bicyclo[3.2.1]oct-7-ylmethyl ester

: 93367-14-7
(2S,3R)-2-benzyloxy-3-hydrazononane

Guidance literature:: Multi-step reaction with 6 steps

1: 76 percent / toluene / 0.5 h / -10 °C

2: K₂CO₃ / methanol / 1 h / 0 °C

3: 94 percent / LiAlH₄ / diethyl ether / 1 h / 0 °C

4: 2.) AlCl₃ / 1.) protection with benzyl ether 2.) CH₂Cl₂, 0 gradC, 1.5 h.

5: 72 percent / Reney-nickel / ethanol / 0.5 h / 20 °C

6: 85 percent / HN₃, Ph₃P, diethyl azodicarboxylate / benzene

With lithium aluminium tetrahydride; aluminium trichloride; tris-(2-chloro-ethyl)-amine; potassium carbonate; triphenylphosphine; diethylazodicarboxylate; Reney-nickel; In methanol; diethyl ether; ethanol; toluene; benzene;
DOI:10.1016/S0040-4039(00)83984-2