[(6-phenyl-4-(p-methylbenzoate)-2,2'-bipyridyl(-1H))PtCl]

Base Information

Chemical Name:[(6-phenyl-4-(p-methylbenzoate)-2,2'-bipyridyl(-1H))PtCl]
CAS No.:1114963-96-0
Molecular Formula:C₂₄H₁₇ClN₂O₂Pt
Molecular Weight:595.944
Hs Code.:

Synonyms:[(6-phenyl-4-(p-methylbenzoate)-2,2'-bipyridyl(-1H))PtCl]

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Chemical Property of [(6-phenyl-4-(p-methylbenzoate)-2,2'-bipyridyl(-1H))PtCl]

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Technology Process of [(6-phenyl-4-(p-methylbenzoate)-2,2'-bipyridyl(-1H))PtCl]

There total 2 articles about [(6-phenyl-4-(p-methylbenzoate)-2,2'-bipyridyl(-1H))PtCl] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: dichlorobis(dimethyl sulfoxide)platinum(II)

: 1114963-94-8
6-phenyl-4-(p-methylbenzoate)-2,2'-bipyridyl

: 1114963-96-0
[(6-phenyl-4-(p-methylbenzoate)-2,2'-bipyridyl(-1H))PtCl]

Guidance literature:: In chloroform; Pt complex added to a soln. of ligand, refluxed for ca 24 h under N2; filtered, rinsed with cold CHCl3 and Et2O; elem. anal.;
DOI:10.1021/ic801767q

Reference yield: 43.0%

: 10025-99-7
potassium tetrachloroplatinate(II)

: 1114963-94-8
6-phenyl-4-(p-methylbenzoate)-2,2'-bipyridyl

: 1114963-96-0
[(6-phenyl-4-(p-methylbenzoate)-2,2'-bipyridyl(-1H))PtCl]

Guidance literature:: In methanol; water; acetonitrile; an aq. soln. of K2PtCl4 added to a suspn. of ligand in MeCN/MeOH, refluxed under N2 for ca 20 h; allowed to cool to room temp., filtered, rinsed with MeOH and Et2O;
DOI:10.1021/ic801767q

Reference yield: 96.0%

: 1114963-96-0
[(6-phenyl-4-(p-methylbenzoate)-2,2'-bipyridyl(-1H))PtCl]

: 536-74-3
phenylacetylene

: 1155358-85-2
[Pt(phenylacetylenide)(6-phenyl-4-(p-MeOCOC₆H₄)-2,2'-bipyridyl(-H))]

Guidance literature:: With N(CH₂CH₃)3; copper(l) iodide; In N,N-dimethyl-formamide; addn, of anhyd. DMF and mine deriv. to mixt. of platinum compd., CuI andphenylacetylene, sonication, degassing with N2, stirring at room temp. for 2.5 d in dark; filtration, washing with diethyl ether, drying, elem. anal.;
DOI:10.1021/ic801947v