phenyl (E)-(1-propenyl) selenide

Base Information

Chemical Name:phenyl (E)-(1-propenyl) selenide
CAS No.:68001-61-6
Molecular Formula:C₉H₁₀Se
Molecular Weight:197.138
Hs Code.:

Synonyms:phenyl (E)-(1-propenyl) selenide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl (E)-(1-propenyl) selenide

Chemical Property:

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Technology Process of phenyl (E)-(1-propenyl) selenide

There total 8 articles about phenyl (E)-(1-propenyl) selenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 590-14-7
1-bromo-1-propene

: 34837-55-3
Phenylselenyl bromide

: 68001-61-6,68001-62-7,14370-96-8
phenyl (1-propenyl) selenide

Guidance literature:: 1-bromo-1-propene; With magnesium; In tetrahydrofuran; for 2h; Reflux; Inert atmosphere;

Phenylselenyl bromide; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ja506031h

Reference yield:

: 14370-82-2
allyl phenyl selenide

: 68001-61-6
phenyl (E)-(1-propenyl) selenide

: 68001-62-7
phenyl (Z)-(1-propenyl) selenide

Guidance literature:: With 18-crown-6 ether; potassium hydroxide; In benzene; at 20 ℃; for 24h; optical yield given as %de; chemoselective reaction;
DOI:10.1016/j.tet.2012.05.027

Reference yield:

: 590-14-7
1-bromo-1-propene

: 23974-72-3
sodium phenylselenide

: 68001-61-6
phenyl (E)-(1-propenyl) selenide

: 68001-62-7
phenyl (Z)-(1-propenyl) selenide

Guidance literature:: With (2,2'-bipyridine)nickel(II) dibromide; In ethanol; at 120 ℃; for 6h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/jo00356a024