C₄₅H₇₄O₈Si₃

Base Information

Chemical Name:C₄₅H₇₄O₈Si₃
CAS No.:1310025-43-4
Molecular Formula:C₄₅H₇₄O₈Si₃
Molecular Weight:827.334
Hs Code.:

C<sub>45</sub>H<sub>74</sub>O<sub>8</sub>Si<sub>3</sub>

Synonyms:C₄₅H₇₄O₈Si₃

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Chemical Property of C₄₅H₇₄O₈Si₃

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Technology Process of C₄₅H₇₄O₈Si₃

There total 17 articles about C₄₅H₇₄O₈Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 994-30-9
triethylsilyl chloride

: C₃₉H₆₀O₈Si₂

: 1310025-43-4
C₄₅H₇₄O₈Si₃

Guidance literature:: With 1H-imidazole; In dichloromethane; at 0 ℃;
DOI:10.1002/cbic.201700655

Reference yield: 88.0%

: C₄₆H₇₆O₈Si₃

: 1310025-43-4
C₄₅H₇₄O₈Si₃

Guidance literature:: C₄₆H₇₆O₈Si₃; With trimethyltin(IV) hydroxide; In toluene; at 85 ℃;

With dmap; acetic anhydride; at 0 ℃;

In water; at 0 - 20 ℃;
DOI:10.1126/science.aan7969

Reference yield:

: 1310025-34-3
C₃₄H₄₄O₅Si

: 1310025-43-4
C₄₅H₇₄O₈Si₃

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran; N,N-dimethyl-formamide / 0.03 h / Inert atmosphere; Cooling with ice

1.2: 0.33 h / 0 °C / Inert atmosphere

2.1: n-butyllithium; diisopropylamine / tetrahydrofuran; pentane / 0.23 h / -78 - 0 °C / Inert atmosphere

2.2: 0.77 h / -78 °C / Inert atmosphere

2.3: -78 °C

3.1: pyridinium p-toluenesulfonate / 3 h / 45 °C / Inert atmosphere

4.1: sodium tetrahydroborate; ethanol / 15 h / -15 °C / Inert atmosphere

5.1: 1H-imidazole / dichloromethane / 2 h / 20 °C / Inert atmosphere

6.1: magnesium / diethyl ether / Inert atmosphere; Reflux

6.2: 1.22 h / -78 °C / Inert atmosphere

6.3: 70 h / 20 °C / Inert atmosphere

7.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.68 h / Inert atmosphere; Cooling with ice

8.1: lithium dihydronaphthylide radical / tetrahydrofuran / 1 h / -30 - -10 °C / Inert atmosphere

9.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / water; acetonitrile / 1.33 h / 20 °C / Inert atmosphere

9.2: 0.75 h / Inert atmosphere; Cooling with ice

10.1: dmap / dichloromethane / 0.25 h / Inert atmosphere; Cooling with ice

With 1H-imidazole; dmap; sodium tetrahydroborate; n-butyllithium; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; ethanol; [bis(acetoxy)iodo]benzene; sodium hexamethyldisilazane; pyridinium p-toluenesulfonate; lithium dihydronaphthylide radical; magnesium; diisopropylamine; In tetrahydrofuran; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; pentane;
DOI:10.1021/ja203034k