(2S,3R)-2-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-6-methyl-hept-4-ynal

Base Information

Chemical Name:(2S,3R)-2-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-6-methyl-hept-4-ynal
CAS No.:160840-62-0
Molecular Formula:C₂₁H₃₂O₃Si
Molecular Weight:360.569
Hs Code.:

Synonyms:(2S,3R)-2-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-6-methyl-hept-4-ynal

Suppliers and Price of (2S,3R)-2-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-6-methyl-hept-4-ynal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R)-2-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-6-methyl-hept-4-ynal

Chemical Property:

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Technology Process of (2S,3R)-2-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-6-methyl-hept-4-ynal

There total 10 articles about (2S,3R)-2-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-6-methyl-hept-4-ynal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 160840-61-9
S-tert-Butyl (2S,3R)-2-(benzyloxy)-3-<(tert-butyldimethylsilyl)oxy>-6-methyl-4-heptynethioate

: 160840-62-0
(2S,3R)-2-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-6-methyl-hept-4-ynal

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; at -78 ℃;
DOI:10.1016/0040-4039(94)85036-4

Reference yield:

: 15787-92-5
4-methyl-2-pentyn-1-ol

: 160840-62-0
(2S,3R)-2-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-6-methyl-hept-4-ynal

Guidance literature:: Multi-step reaction with 5 steps

3: 86 percent / HSiCl₃, Et₃N / benzene / Ambient temperature

4: 95 percent / imidazole / dimethylformamide / 0.5 h / Ambient temperature

5: DIBALH / CH₂Cl₂; toluene / 0.5 h / -78 °C

With 1H-imidazole; trichlorosilane; diisobutylaluminium hydride; triethylamine; In dichloromethane; N,N-dimethyl-formamide; toluene; benzene;
DOI:10.1021/jo00123a030

Reference yield:

: 133756-18-0
S-tert-butyl 2-(benzyloxy)ethanethioate

: 160840-62-0
(2S,3R)-2-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-6-methyl-hept-4-ynal

Guidance literature:: Multi-step reaction with 5 steps

3: 86 percent / HSiCl₃, Et₃N / benzene / Ambient temperature

4: 95 percent / imidazole / dimethylformamide / 0.5 h / Ambient temperature

5: DIBALH / CH₂Cl₂; toluene / 0.5 h / -78 °C

With 1H-imidazole; trichlorosilane; diisobutylaluminium hydride; triethylamine; In dichloromethane; N,N-dimethyl-formamide; toluene; benzene;
DOI:10.1021/jo00123a030