Technology Process of C29H25N7O4
There total 10 articles about C29H25N7O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylamine;
In
dichloromethane;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 9 steps
1.1: sodium hydrogencarbonate / ethanol / 4 h / 20 °C
2.1: N-iodo-succinimide / N,N-dimethyl-formamide / 4 h / 20 °C
3.1: bis-triphenylphosphine-palladium(II) chloride / toluene / 27 h / 110 °C
3.2: 16 h / 20 °C
4.1: 1-methyl-pyrrolidin-2-one / 1.5 h / 90 °C
5.1: potassium carbonate / 1-methyl-pyrrolidin-2-one / 65 h / 97 °C
6.1: water; sodium nitrite; acetic acid / 0.75 h / 60 °C
6.2: 0 °C / pH 7
7.1: trichlorophosphate / 5 h / 80 °C
7.2: 20 °C / pH 11
8.1: isopropyl alcohol / 70 °C
8.2: 48 h / 70 °C
9.1: triethylamine / dichloromethane / 20 °C
With
N-iodo-succinimide; water; sodium hydrogencarbonate; potassium carbonate; acetic acid; triethylamine; sodium nitrite; trichlorophosphate;
bis-triphenylphosphine-palladium(II) chloride;
In
1-methyl-pyrrolidin-2-one; ethanol; dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol; toluene;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: N-iodo-succinimide / N,N-dimethyl-formamide / 4 h / 20 °C
2.1: bis-triphenylphosphine-palladium(II) chloride / toluene / 27 h / 110 °C
2.2: 16 h / 20 °C
3.1: 1-methyl-pyrrolidin-2-one / 1.5 h / 90 °C
4.1: potassium carbonate / 1-methyl-pyrrolidin-2-one / 65 h / 97 °C
5.1: water; sodium nitrite; acetic acid / 0.75 h / 60 °C
5.2: 0 °C / pH 7
6.1: trichlorophosphate / 5 h / 80 °C
6.2: 20 °C / pH 11
7.1: isopropyl alcohol / 70 °C
7.2: 48 h / 70 °C
8.1: triethylamine / dichloromethane / 20 °C
With
N-iodo-succinimide; water; potassium carbonate; acetic acid; triethylamine; sodium nitrite; trichlorophosphate;
bis-triphenylphosphine-palladium(II) chloride;
In
1-methyl-pyrrolidin-2-one; dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol; toluene;