3,5-dichlorobenzenesulfinic acid

Base Information

• Chemical Name: 3,5-dichlorobenzenesulfinic acid
• CAS No.: 62617-38-3
• Molecular Formula: C₆H₄Cl₂O₂S
• Molecular Weight: 211.069

Synonyms:3,5-dichlorobenzenesulfinic acid

Chemical Property of 3,5-dichlorobenzenesulfinic acid

Chemical Property:

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Technology Process of 3,5-dichlorobenzenesulfinic acid

There total 1 articles about 3,5-dichlorobenzenesulfinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

3,5-dichlorobenzensulfonyl chloride (705-21-5) → 3,5-dichlorobenzenesulfinic acid (62617-38-3)

Guidance literature:

With triethylamine; para-thiocresol; In dichloromethane; at -76 ℃; for 0.25h;

DOI:10.1055/s-1990-26884

Reference yield: 81.0%

2-Chloroquinoline (612-62-4) + 3,5-dichlorobenzenesulfinic acid (62617-38-3) → 2-((3,5-dichlorophenyl)sulfonyl)quinoline

Guidance literature:

In neat (no solvent); at 20 ℃; Milling; Green chemistry;

DOI:10.1039/d1gc02015c

Reference yield: 76.0%

Quinoline N-oxide (1613-37-2) + 3,5-dichlorobenzenesulfinic acid (62617-38-3) → 2-((3,5-dichlorophenyl)sulfonyl)quinoline

Guidance literature:

With Eosin Y; In water; acetone; at 20 ℃; for 12h; Irradiation;

DOI:10.1039/c9gc01175g

upstream raw materials:

3,5-dichlorobenzensulfonyl chloride

Downstream raw materials:

3,5-Dichloro-benzenesulfinic acid; compound with 2-benzyl-isothiourea

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